Electrochemical Synthesis of Nitro-Chitosan and Its Performance in Chromium Removal
Abstract
:1. Introduction
2. Results and Discussion
2.1. Electrodeposition
2.2. Characterization
Peak (cm−1) | Assignment |
---|---|
1663 | combination of amide I C=O stretching, asymmetric NO2 stretching and OH deformation vibrations |
1585 | NH bending frequency |
1442 | C–C stretching vibration |
1380 | combination of CH3 deformation and CO stretching frequencies |
1203 | combination of NH deformation and symmetric NO2 stretching vibrations |
1154, 1020 | symmetric and asymmetric stretching vibrations of C–O–C respectively |
970 | amine oxide |
805 | O–H deformation |
2.3. Equilibrium Adsorption Isotherms
2.4. Effect of pH on Adsorption of Chromate
2.5. Sorption Kinetics
3. Experimental Section
3.1. Electrodeposition of Chitosan
3.2. FTIR
3.3. Raman Spectroscopy
3.4. XPS
3.5. Absorption Experiments
3.6. DCP-AES
4. Conclusions
Acknowledgments
Conflict of Interest
References
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Jha, P.K.; Halada, G.P.; McLennan, S.M. Electrochemical Synthesis of Nitro-Chitosan and Its Performance in Chromium Removal. Coatings 2013, 3, 140-152. https://doi.org/10.3390/coatings3030140
Jha PK, Halada GP, McLennan SM. Electrochemical Synthesis of Nitro-Chitosan and Its Performance in Chromium Removal. Coatings. 2013; 3(3):140-152. https://doi.org/10.3390/coatings3030140
Chicago/Turabian StyleJha, Prashant K., Gary P. Halada, and Scott M. McLennan. 2013. "Electrochemical Synthesis of Nitro-Chitosan and Its Performance in Chromium Removal" Coatings 3, no. 3: 140-152. https://doi.org/10.3390/coatings3030140
APA StyleJha, P. K., Halada, G. P., & McLennan, S. M. (2013). Electrochemical Synthesis of Nitro-Chitosan and Its Performance in Chromium Removal. Coatings, 3(3), 140-152. https://doi.org/10.3390/coatings3030140