1. Introduction
Glass Fiber-Reinforced Plastic (GFRP) pipes are widely used in various industries due to their exceptional mechanical properties, corrosion resistance, and durability [
1]. These materials are particularly favored in environments where conventional materials like steel may suffer from rapid degradation due to aggressive environmental factors [
2,
3,
4]. GFRP pipes support sustainable development by reducing maintenance needs and extending service life, particularly in challenging conditions, which conserves resources and minimizes environmental impact. However, to ensure the long-term reliability of GFRP pipes, it is very important to accurately characterize their mechanical properties, particularly under the influence of environmental factors such as temperature, humidity, and chemical exposure.
The mechanical properties of GFRP pipes, particularly their circumferential (hoop) strength, are essential for their application in various industries, including water supply, chemical processing, and oil and gas transportation. Several methods exist for evaluating the circumferential tensile properties of composite products, including the hydrostatic pressure test, flat crush test, segment-type ring burst test, ring burst test, and split-disk test [
5]. Unlike the hydrostatic burst test, which requires testing the entire product, the split-disk test offers distinct advantages, such as simplicity, cost-effectiveness, and higher efficiency [
5]. The split-disk method has emerged as a standard technique for evaluating these properties. This method involves subjecting a ring or disk cut from the pipe to a diametrical compression, providing valuable insights into the material’s hoop strength and failure characteristics. Numerous studies [
5,
6,
7,
8,
9,
10,
11,
12,
13] have explored different aspects of this testing method, each contributing to a more nuanced understanding of composite materials’ behavior under various conditions, including the influence of aggressive environments [
2,
14,
15,
16,
17,
18].
The exploration of mechanical testing methods is a central theme in the study of composite materials. Zhao et al. [
5] used the split-disk test for measuring filament-wound composites’ mechanical properties using 3D Digital Image Correlation and finite element modeling, finding that friction between the ring and disk significantly affects the strain measurements and identifying a low strain zone at the ring split due to local bending. In a similar work, Kaynak et al. [
6] investigated the split polymer test method, focusing on the behavior of polymer composites under stress, exploring how different processing parameters affect continuous fiber-reinforced epoxy composite tubes produced by filament winding. Their findings revealed that the type of epoxy resin had little effect on the performance, while carbon fibers and winding angles greater than 60° significantly improved the tubes’ strength. Both studies underscore the importance of split-disk techniques in advancing the understanding of material behavior under conditions that mimic real-world scenarios.
Furthermore, these findings align with the work of Sapozhnikoy et al. [
7] and Dick and Korkolis [
8], who concentrated on the mechanical measurements in polymer and tubular materials, respectively.
The study presents [
19] a method for characterizing filament-wound composite pipes using glass/vinylester and carbon/epoxy materials. Tubular samples were tested through a split-disk and a newly designed biaxial test, which minimized the stress concentration and ensured alignment. An optical technique assessed the void content, and failure envelopes in the σ2 − τ12 plane were obtained and compared with common failure theories. The Puck criterion accurately predicted failure, especially under combined torsional and compressive loads. Another study [
10] uses finite element analysis to explain why split-disk tests yield lower FRP rupture strains than flat coupon tests. It was found that geometric discontinuities and bending at the FRP ring gap increased local strains, leading to earlier rupture. Additionally, the effects of adhesive properties, FRP stiffness, overlap geometry, and friction were examined, further elucidating the behavior of these materials.
Further examining composite structures, Benyahia et al. [
11] investigated thick, ±55° filament-wound glass/epoxy tubes for offshore applications using quasi-static tests. They developed a redesigned fixture system that reduced the edge stress concentration during split-disk tensile tests on pipes with an 86 mm diameter and a thickness of 6.2 mm. Testing both notched and unnotched specimens revealed that increased notch size and number reduced the yield stress and increased the yield strain, negatively impacting the structural integrity.
Another paper [
12] focused on stress and strain distribution in the longitudinal and circumferential directions of glass–polyester composite pipes under tensile testing, widely used in chemical and process industries. Tension tests on flat samples and rings from ±55° filament-wound pipes determined the tensile strengths in both directions.
A modified split-disk test (ASTM D 2290 [
20]) was considered in [
13] to assess the stress–strain behavior of two GFRP rings using a simple specimen preparation method. GFRP-confined glass fiber rings of 1.75 mm, 2.50 mm, and 3.25 mm thicknesses, wrapped with E-glass and S-glass fabrics, underwent uni-axial tensile testing. The results for the E-glass composites were compared to those of the S-glass composites. Finite element simulations of selected specimens were also conducted by the authors, yielding strain efficiency factors that align well with the experimental data for design applications.
A significant focus of research in the specialized literature is the effect of environmental exposure on the degradation mechanisms of FRP materials. Silva et al. [
21] investigated the degradation of GFRP laminates under accelerated aging, highlighting the challenges in predicting long-term degradation, particularly under salt fog exposure. The authors of the paper [
17] explored the impact of accelerated thermal and hydrothermal aging on E-glass fiber-reinforced epoxy resin composite pipes, emphasizing how hydrothermal conditions severely affect the mechanical properties. Mahmoud and Tantawi [
15] studied the effects of strong acids on glass–polyester GRP pipes, demonstrating the detrimental effects of acidic environments on mechanical performance. Additionally, research on the tensile properties of glass–polyester pipes exposed to various acidic and alkaline solutions [
16] found that alkaline exposure led to a significant reduction in the tensile properties, particularly with higher alkalinity, while acid treatments improved properties such as the tensile strength and elasticity. The study also observed substantial changes in weight, impact resistance, flexural strength, and hardness in glass–polyester GRP pipes exposed to strong acids, with sulfuric acid causing the most significant loss in strength, as revealed by X-ray diffraction analysis. Similarly, Bi et al. [
22] used acoustic emission techniques to investigate aging damage in GFRP pipes subjected to acidic conditions and external mechanical loads, identifying matrix cracking and delamination as primary degradation mechanisms. Zhang and Deng [
23] applied molecular dynamics simulations to study GFRP degradation in seawater, showing reductions in the Young’s modulus and interlaminar strength with increasing seawater content and temperature.
The present study presents a significant advancement in understanding the mechanical properties of GFRP pipes by investigating their behavior in the circumferential direction using the split-disk method, particularly under aggressive environmental conditions. Unlike previous studies, this research emphasizes the effects of exposure to saltwater and alkaline solutions at elevated temperatures, which are critical factors in real-world applications of GFRP pipes. By determining the key mechanical properties such as the hoop tensile strength, elastic modulus, and Poisson’s ratio, this study highlights how these properties are affected by environmental degradation. Importantly, the research incorporates rigorous statistical analysis and finite element analysis to evaluate the correlations between the ultimate tensile strength, elastic modulus, and Poisson’s ratio, providing a comprehensive understanding of the mechanical behavior of GFRP pipes under different conditions.
By examining how these environmental conditions degrade critical properties such as the hoop tensile strength, elastic modulus, and Poisson’s ratio, this study provides essential data for designing GFRP systems with extended service life in harsh conditions. This research not only identifies degradation patterns but also supports sustainable infrastructure by informing maintenance strategies and material choices that reduce environmental impact through longer-lasting installations. Therefore, this study contributes to sustainable development by supporting the design and selection of materials that enhance the resilience and longevity of industrial infrastructure.
2. Materials and Methods
2.1. Samples and Immersion Conditions
The tested samples consisted of a Glass Fiber-Reinforced Epoxy (GRE) pipe with an internal diameter of 81 mm and a wall thickness of 4 mm. The specimens were cut to have the geometrical characteristics presented in
Figure 1, according to standard [
20]. For each experimental condition, three replicate specimens were tested to account for variability and ensure the reproducibility of results.
The immersing solutions were selected to reflect significant differences in the pH as seen in
Table 1. Their pH values were measured using the MULTI 9630 pH meter. The alkaline solution was prepared following CSA S806 [
24], containing 118.5 g of Ca(OH)
2, 0.9 g of NaOH, and 4.2 g of KOH per liter of water, while the other environment consisted of a 3.5% sodium chloride (NaCl) solution.
In order to analyze the effect of the temperature on the mechanical behavior of GFRP pipes, some specimens were inserted in an oven at a constant temperature of 50 °C, as shown in
Figure 2. To ensure accurate and consistent experimental conditions, both the pH and temperature were carefully controlled throughout the study. The pH of the immersion solutions, including the saltwater and alkaline solutions, was monitored and the pH level was kept within a narrow range (±10%) to ensure that chemical reactions affecting the degradation of the GFRP pipes occurred consistently across all specimens. Fluctuations outside this range were minimized by frequent adjustments to the solutions.
2.2. Design of Experiments
The Design of Experiment (DoE) and Analysis of Variance (ANOVA) techniques utilize arrays to systematically organize the factors influencing the behavior of the GFRP material and the corresponding levels at which they should be configured. A full factorial design was implemented, comprising six experimental conditions to examine the effects of the temperature (20 °C and 50 °C) and environment (air, saltwater, and alkaline solution). The testing conditions are detailed in
Table 2.
2.3. Mechanical Testing
The test fixture, illustrated in
Figure 3 and produced using a lathe machine, consists of two semicircular metal plates (D-blocks) connected to the upper and lower arms of the fixture with pins. During testing, the bending moment generated at the junction of the split-disk test fixtures primarily affects the apparent tensile strength rather than the true tensile strength of each test [
13]. Consequently, the test fixture was specifically designed to minimize the influence of this bending moment.
The experimental tests were carried out using the Walter Bai LF300 Walter+Bai AG, (Löhningen, Switzerland) universal testing machine with the capacity of 300 kN, as shown in
Figure 4, at a constant strain rate of 3 mm/min. All tests were performed at room temperature. The data were continuously monitored by the computer and data acquisition system until the specimen attained its ultimate tensile strength (UTS) and subsequently fractured.
The ultimate tensile strength was determined with the formula (1) [
20]:
where
F—measured force, N;
A—section area in the calibrated area, mm
2;
b—width in the calibrated area, mm;
t—pipe wall thickness, mm.
The tensile testing machine measured the force, F, necessary for the calculation of the tensile strength in the circumferential direction.
The procedure followed during the split-disk tests involved several key steps to ensure accurate measurements and results. Firstly, the reduced section dimensions of the specimens were measured using digital calipers. Thickness measurements were taken at four points on each specimen, two of which were located in the gauge sections, while the width of the reduced sections was also recorded. These measurements allowed for the calculation of the reduced section areas, using the minimum thickness and width values.
Next, the specimens were mounted onto the split-disk test fixture, ensuring that the reduced sections were aligned with the split in the fixture. Once mounted, the testing machine was set to a constant loading rate, and the test was initiated. During the test, load and strain data were continuously recorded until the specimen failed. These data were then used to generate stress–strain curves for each specimen. After the tests, the ultimate hoop tensile strength and hoop tensile modulus values were calculated by averaging the measurements from all specimens in each test group. Standard deviations were also computed and reported to reflect the variability within the test groups, providing a comprehensive understanding of the material’s performance under the tested conditions.
To determine the Poisson’s ratio for the investigated samples, strain gauges were attached to the surface of each specimen in two directions to measure both longitudinal (
εx) and transverse strains (
εy), as illustrated in
Figure 5a. The strain gauges used had a gauge factor of
k = 2.19 and a resistance of 350 Ω, with data recorded using the MGCplus acquisition system (
Figure 5b).
The uncertainty range for each measured property was calculated using the standard deviation of the measured values. For each experimental condition, three measurements were taken, and the standard deviation was determined to quantify variability. This approach provides a statistical representation of the uncertainty associated with the measurements.
Hooke’s law for an orthotropic material in a system of rectangular Cartesian coordinates with axes perpendicular to the planes of symmetry of elastic characteristics can be conveniently represented in matrix form [
25]:
aij—components of the flexibility matrix.
The components of the tensor can be expressed in terms of technical constants:
where
Ex, Ey, Ez—elastic moduli;
νxy, νyx, νzx, νxz, νzy, νyz—Poisson’s ratios;
Gxy, Gyz, Gzx—shear moduli.
In the performed experiment, there is only circumferential stress (denoted ).
Circumferential strain (denoted ) and axial strain (denoted ) were measured.
The ratio of measured strains gives one Poisson’s ratio:
But there is the following relation:
2.4. Theoretical Analysis of the Stress State in the Zone of Circular Notches
The presence of circular notches in the tested specimens leads to distortion of the homogeneous stress state and the occurrence of stress concentration. This phenomenon is important to consider when establishing the strength limits of composite pipe material. In addition, theoretical analysis allows us to establish a complete picture of stress and strain distribution in the stress concentration zone. Comparison with the results of the experimental measurements of strains in the zone of installation of strain gauges is important to verify the results of the study. When conducting experiments on the strain measurement, strain gauges with dimensions of 8 × 8 mm were used. At significant values of strain gradients, the sensor readings correspond to some average strain values. The theoretical study makes it possible to determine a detailed picture of strain distribution within the area of sensor installation. In addition, theoretical analysis makes it possible to predict the value of stresses at the points of their maximum concentration. Taking into account the stress concentration caused by the presence of semicircular notches is necessary for the reasonable application of the results of the study to analyze the strength of pipes without holes.
For theoretical analysis of the stress concentration zone, the section of the specimen in the vicinity of the hole is considered. Due to the symmetry with respect to the axes oh and ou, it is sufficient to consider the fourth part shown in
Figure 6.
When analyzing this problem, the pipe material is considered as a homogeneous orthotropic elastic body. The mathematical formulation of the problem is reduced to the following complete system of equations [
26]:
In physical relations (22): Ex, Ey—modulus of elasticity in axial and circumferential directions, respectively; νxy, νyx—Poisson’s ratios; Gxy—shear module.
On two lines, x = 0, y = 0, symmetry conditions are set on the boundary y = h and a uniform tensile stress corresponding to the applied load during tests is set. The other boundaries are free from external loads.
The complete system of Equations (15) and (16) can be reduced to the equivalent two solving equations with respect to displacements. The physical relations (20…22) in the inverse form are as follows:
After replacing deformations in physical relations (23) by displacements using (17) and (18), the equations of equilibrium (15) and (16) are reduced to the following solving equations with respect to displacements:
The solution of boundary value problems for areas of complex shape is possible using approximate methods. In this paper, the finite element method is used, which allows us to find numerical solutions with accuracy sufficient for practical applications. The calculations were conducted in the ANSYS v.2020 R1 program complex in the framework of static analysis. For discretization of the problem, a plane 6-node element PLANE183 with the option “plane stress state” was used. The approximation of displacements u and v within the finite element is given by quadratic functions. The finite element model shown in
Figure 7, which utilizes model symmetry to optimize computation, consists of 2717 nodes and 1306 triangular elements. This symmetry allowed for a more efficient setup, minimizing the node and element count while preserving accuracy in stress distribution and deformation predictions.
The elastic material properties of the orthotropic material were specified according to the experimental results obtained for the specimen that was kept in air at 20 °C. The calculations were performed for a nominal tensile stress of 100 MPa on line y = h.
4. Conclusions
The present study provides important insights into the degradation of GFRP pipes under varying environmental conditions, with a particular focus on the impact of the temperature and corrosive agents. The findings demonstrate that GFRP pipes are highly susceptible to mechanical degradation when exposed to elevated temperatures and aggressive environments like saltwater and alkaline solutions. Exposure to saltwater causes a significant decrease in the ultimate tensile strength (UTS) and elastic modulus as the temperature rises, with a notable reduction at 50 °C. This leads to diminished resistance to deformation, reduced stiffness, and lower ductility, making the material more brittle. Similarly, this study shows that alkaline environments, particularly at high temperatures, result in even more severe degradation of GFRP, significantly reducing both the strength and stiffness.
In contrast, exposure to air at 50 °C results in only moderate reductions in the UTS and elastic modulus, with the Poisson’s ratio remaining relatively stable. This suggests that, in the absence of corrosive agents, GFRP pipes retain much of their stiffness and ductility, even at elevated temperatures. These results highlight the importance of considering environmental factors such as the pH and the composition of the environment when assessing the long-term durability of GFRP pipes.
This study also emphasizes that combined environmental factors, especially the temperature and solution type, have a synergistic effect on the mechanical degradation of GFRP pipes. Exposure to both saltwater and alkaline environments at elevated temperatures proves to be more detrimental than exposure to individual factors alone.
While this study provides valuable insights, there are limitations. The experimental setup focused primarily on saltwater, alkaline solutions, and air, excluding other potentially aggressive environments, such as acidic solutions. Additionally, only short-term exposure was considered, and the effects of prolonged exposure remain unclear. Variations in manufacturing processes and material formulations could further influence GFRP pipe performance, meaning the results may not be universally applicable to all types of GFRP materials.
Future research should expand on these findings by investigating a broader range of environmental conditions, including acidic environments and varying concentrations of saltwater and alkaline solutions. Long-term exposure studies will be essential to understanding the degradation mechanisms in real-world applications. Moreover, incorporating other loadings, such as cyclic loading, could offer a more comprehensive view of GFRP performance under practical conditions. Further exploration of GFRP formulations, resin types, and fiber orientations will deepen the understanding of how material composition influences degradation under environmental and thermal loads.