Strength Enhancement of Laser Powder Bed Fusion 316L by Addition of Nano TiC Particles
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials Preparation
2.2. Fabrication
2.3. Tests
3. Results
3.1. Phase Analysis
3.2. Microstructure
3.3. Microhardness
3.4. Tensile Property at Room Temperature
3.5. Tensile Property at High Temperature
4. Discussion
4.1. Strength Enhancement
- (1)
- Dispersion strengthening means that the second-phase particles are distributed in the alloy, which become effective obstacles of dislocation movement. The hardness of the TiC particle is far more than 316L. Their relationship is non-coherent. As such, the dislocation cannot pass through the TiC particle. The movement of dislocation will have to move via an Orowan round, overcoming the reaction force. The strength improvement can be illustrated by the Orowan formula [24]:
- (2)
- For metal-base composite materials, the introduction secondary-phase particles will probably alter the crystalline dynamics of the molten pool. On one hand, some of the nano particles may become the seeds for the crystal. On the other hand, the rest of the nano particles may obstruct the growth of the grain and, thus, can form fine grains. As demonstrated in Figure 6, the average sizes of the grains decreases significantly with the increased content of the TiC addition. According to the Hall–Petch relationship, the improvement of strength caused by grain refinement can be calculated as follows:
- (3)
- The main enhancement mechanism of particle-enhanced composite materials is the transfer of the load from the matrix to the high-strength particle [26]. In other words, the high-strength particles undertake much of the load. As can be seen from Figure 9, the TiC particles did not fall of from the matrix of 316L. Based on the tight bonding between TiC and 316L, the nano TiC particles may undertake much of the load. The strength improvement caused by bonding can be calculated as follows:
4.2. Ductility Improvement
5. Conclusions
- (1)
- The 2 wt% TiC/316L sample with near full density was prepared by optimizing the process parameters in LPBF.
- (2)
- The average sizes of grains in the TiC/316L composite decreased with the increased content of TiC.
- (3)
- The tensile properties at both room temperature and at high temperature for the 2 wt% TiC/316L sample were significantly enhanced.
- (4)
- The strength enhancement may attributed to the Orowan mechanism, fine grain strengthening, and load-transferred strengthening.
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Content (wt%) | Time (h) | Speed (rpm) | Milling Time (min) | Dwelling Time (min) |
---|---|---|---|---|
2 | 4 | 120 | 20 | 20 |
4 | 8 | 150 | 20 | 20 |
Content (wt%) | Laser Power (W) | Scan Speed (mm/s) | Layer Thickness (μm) | Hatch Distance (μm) |
---|---|---|---|---|
0 | 180 | 1000 | 30 | 60 |
2 | 200 | 1000 | 30 | 60 |
4 | 240 | 800 | 30 | 60 |
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Liu, Y.; Xie, D.; Lv, F. Strength Enhancement of Laser Powder Bed Fusion 316L by Addition of Nano TiC Particles. Materials 2024, 17, 1129. https://doi.org/10.3390/ma17051129
Liu Y, Xie D, Lv F. Strength Enhancement of Laser Powder Bed Fusion 316L by Addition of Nano TiC Particles. Materials. 2024; 17(5):1129. https://doi.org/10.3390/ma17051129
Chicago/Turabian StyleLiu, Yanyan, Deqiao Xie, and Fei Lv. 2024. "Strength Enhancement of Laser Powder Bed Fusion 316L by Addition of Nano TiC Particles" Materials 17, no. 5: 1129. https://doi.org/10.3390/ma17051129