Non-Newtonian Flow Characteristics of Heavy Oil in the Bohai Bay Oilfield: Experimental and Simulation Studies
Abstract
:1. Introduction
2. Methodology
2.1. Physical Experiments
2.1.1. Rheology Test
2.1.2. TPG Measurement and Its Critical Condition
- Experimental devices were connected according to the flow chart.
- The temperature of the thermotank was set to 30 °C, and the core with the saturated water was required to stand for at least 24 h.
- The heavy oil sample was used to displace the water in the core at a flow rate of 0.05 mL/min after bypassing the oil column tube #1. The displacing flow rate was increased to 0.5 mL/min when the water cut at the outlet was lower than 2% until the volume of injected heavy oil sample reached ten times the pore volume (PV) of the core, and there was no water production.
- The ISCO pump was stopped, and the height of the oil column in the oil column tube #2 was lowered to about 5 cm.
- The oil column tube #1 was put into use. The height of the oil column in the oil column tube #1 was raised to the same height as that in the oil column tube #2 by restarting the ISCO pump with the flow rate of 0.02 mL/min. The ISCO pump was stopped again, and this condition was kept for 24 h.
- The flow rate of 0.002 mL/min was used to displace and the height of the oil column in the oil column tube #1 increased gradually. The pressure gradient was the TPG of the heavy oil sample when the height of the oil column in the oil column tube #2 began to move.
- The TPG under the and was measured, where was the permeability, which started from , and is the viscosity, which started from .
- If the TPG existed under the and , a smaller than was used to replace and the TPG at the and was measured. If not, a larger than was used.
- The selection of was repeated until two cases for the inexistence of the TPG and four cases for the existence of the TPG were obtained. A curve of the relationship between the TPGs greater than 0 MPa/m and the corresponding viscosity was drawn. The intercept of the fitting curve on the viscosity axis was considered to be the critical viscosity () at the . Here, the TPG would be present for the specific permeability when the viscosity is higher than the critical viscosity (). Otherwise, the TPG no longer existed.
- The above steps were repeated until sets of permeability and the corresponding critical viscosities were obtained, where was determined by the requirements of the study.
2.1.3. Flow Experiments
2.2. Numerical Method
2.2.1. Corrected Darcy’s Law
2.2.2. Flow Model
- The corrected Darcy’s law of Equation (2) was applied.
- The model was 3D with two phases (the oil and water phases).
- The water component existed only in the water phase, which did not exchange its mass with the oil phase.
- The reservoir rock was compressible and anisotropic, while the fluid was compressible.
- The effects of the capillary force and gravity were taken into account.
2.2.3. IMPES
3. Results and Discussion
3.1. Rheology of Heavy Oil
3.2. Threshold Pressure Gradient (TPG)
3.2.1. Impact of Flow Rate on TPG Measurement
3.2.2. Relationship between TPG and Mobility
3.3. Flow Characteristics of Heavy Oil in Porous Media
3.4. Simulation
3.4.1. Validation
3.4.2. TPG Sensitivity
4. Conclusions
Acknowledgments
Author Contributions
Conflicts of Interest
References
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Parameters | Heavy Oil Samples | ||||||
---|---|---|---|---|---|---|---|
#1 | #2 | #3 | #4 | #5 | #6 | ||
Composition, mol.% | C3 | 0.12 | 0.09 | 0.03 | 0.01 | 0.00 | 0.00 |
i-C4 | 0.21 | 0.15 | 0.06 | 0.04 | 0.00 | 0.00 | |
n-C4 | 0.50 | 0.30 | 0.14 | 0.09 | 0.00 | 0.00 | |
i-C5 | 0.82 | 0.54 | 0.32 | 0.23 | 0.00 | 0.00 | |
n-C5 | 0.71 | 0.43 | 0.25 | 0.16 | 0.00 | 0.00 | |
C6 | 0.50 | 0.33 | 0.24 | 0.16 | 0.00 | 0.00 | |
C7 | 0.88 | 0.77 | 0.74 | 0.67 | 0.00 | 0.00 | |
C8 | 3.34 | 2.98 | 2.81 | 2.63 | 0.24 | 0.34 | |
C9 | 5.90 | 5.82 | 5.88 | 5.83 | 1.87 | 2.11 | |
C10 | 17.65 | 18.42 | 18.88 | 19.07 | 13.12 | 13.97 | |
C11 | 25.52 | 26.66 | 26.76 | 27.40 | 27.46 | 28.53 | |
C12+ | 43.85 | 43.51 | 43.88 | 43.72 | 57.31 | 55.05 | |
Asphaltene content, wt. % | 3.61 | 3.48 | 3.12 | 2.82 | 3.55 | 3.04 | |
Density (30 °C), g/cm3 | 0.96 | 0.93 | 0.90 | 0.86 | 0.95 | 0.88 | |
Viscosity (30 °C), mPa∙s | 783 | 461 | 242 | 129.78 | 586.8 | 218.97 |
Core Number | Length, cm | Dimension, cm | Porosity, % | Permeability, mD | Marks |
---|---|---|---|---|---|
#1 | 25.21 | 2.53 | 21.09 | 363 | Used to study the impact of flow rate on threshold pressure gradient (TPG) measurement. |
#2 | 25.16 | 2.52 | 21.03 | 359 | |
#3 | 25.18 | 2.49 | 21.07 | 360 | |
#4 | 25.16 | 2.52 | 22.06 | 502 | |
#5 | 25.05 | 2.50 | 23.58 | 946 | |
#6 | 25.01 | 2.51 | 20.84 | 324 | Used to study the relationship between TPG and mobility. |
#7 | 25.24 | 2.48 | 24.83 | 1465 | |
#8 | 24.81 | 2.48 | 27.16 | 2765 | |
#9 | 25.30 | 2.50 | 21.57 | 426 | |
#10 | 25.00 | 2.53 | 26.68 | 2465 | |
#11 | 24.92 | 2.51 | 28.56 | 3621 | |
#12 | 24.62 | 2.48 | 21.04 | 361 | |
#13 | 25.29 | 2.52 | 27.37 | 2894 | |
#14 | 24.81 | 2.49 | 28.61 | 3710 | |
#15 | 24.80 | 2.52 | 21.16 | 382 | |
#16 | 25.32 | 2.48 | 27.06 | 2695 | |
#17 | 24.86 | 2.53 | 28.51 | 3580 | |
#18 | 25.07 | 2.49 | 19.37 | 92 | Used to determine the critical viscosity for the existence of TPG at a given permeability. |
#19 | 24.79 | 2.51 | 20.30 | 238 | |
#20 | 25.38 | 2.50 | 21.10 | 367 | |
#21 | 24.67 | 2.48 | 22.92 | 647 | |
#22 | 25.22 | 2.51 | 23.63 | 976 | |
#23 | 25.09 | 2.49 | 24.85 | 1460 | |
#24 | 25.26 | 2.50 | 26.41 | 2289 | |
#25 | 24.96 | 2.51 | 27.52 | 3042 | |
#26 | 24.75 | 2.48 | 28.49 | 3525 | |
#27 | 25.19 | 2.49 | 21.09 | 362 | Used to study the flow characteristics of heavy oil. |
#28 | 25.18 | 2.47 | 21.02 | 358 | |
#29 | 25.21 | 2.52 | 21.05 | 360 | |
#30 | 25.04 | 2.52 | 24.76 | 1452 | |
#31 | 25.00 | 2.51 | 26.37 | 2278 | |
#32 | 25.19 | 2.50 | 21.05 | 362 | |
#33 | 25.17 | 2.48 | 21.03 | 358 | |
#34 | 25.22 | 2.52 | 21.09 | 365 | |
#35 | 25.07 | 2.51 | 24.62 | 1448 | |
#36 | 24.97 | 2.50 | 26.28 | 2270 |
Parameters | Value | |
---|---|---|
Composition, mg/L | Na+ and K+ | 3091.960 |
Ca2+ | 276.17 | |
Mg2+ | 156.68 | |
CO32- | 11 | |
HCO3− | 311.48 | |
SO42− | 85.29 | |
Cl- | 5436.34 | |
TDS | 9374.12 | |
Density (30 °C), g/cm3 | 1.046 |
Flow Rate, mL/min | Threshold Pressure Gradient, MPa/m | ||||
---|---|---|---|---|---|
Core Sample: #1 | Core Sample: #2 | Core Sample: #3 | Core Sample: #4 | Core Sample: #5 | |
Oil Sample: #1 | Oil Sample: #2 | Oil Sample: #3 | Oil Sample: #4 | Oil Sample: #5 | |
0.001 | 0.00127 | 0.00110 | 0.00087 | 0.00114 | 0.00092 |
0.002 | 0.00127 | 0.00110 | 0.00087 | 0.00114 | 0.00092 |
0.003 | 0.00127 | 0.00110 | 0.00087 | 0.00114 | 0.00092 |
0.004 | 0.00133 | 0.00124 | 0.00092 | 0.00126 | 0.00099 |
0.005 | 0.00142 | 0.00140 | 0.00102 | 0.00134 | 0.00109 |
0.006 | 0.00164 | 0.00146 | 0.00103 | 0.00150 | 0.00114 |
0.008 | 0.00171 | 0.00158 | 0.00108 | 0.00162 | 0.00121 |
0.010 | 0.00186 | 0.00168 | 0.00114 | 0.00174 | 0.00128 |
Core | Permeability, mD | Oil Sample | Viscosity, mPa∙s | TPG, MPa/m |
---|---|---|---|---|
#6 | 324 | #1 | 783 | 0.00135 |
#7 | 1465 | #1 | 783 | 0.00083 |
#8 | 2765 | #1 | 783 | 0.00070 |
#9 | 426 | #2 | 461 | 0.00104 |
#10 | 2465 | #2 | 461 | 0.00049 |
#11 | 3621 | #2 | 461 | 0.00046 |
#12 | 361 | #3 | 242 | 0.00083 |
#13 | 2894 | #3 | 242 | 0.00045 |
#14 | 3710 | #3 | 242 | 0.00042 |
#15 | 382 | #4 | 130 | 0.00075 |
#16 | 2695 | #4 | 130 | 0.00034 |
#17 | 3580 | #4 | 130 | 0.00026 |
Layer | Thickness ∆z, m | Depth to Center of Layer, m | Horizontal Permeability, mD | Vertical Permeability, mD | Porosity, Fraction | Initial Pressure, MPa | Initial oil Saturation, Fraction | Initial Water Saturation, Fraction |
---|---|---|---|---|---|---|---|---|
1 (top) | 6.096 | 1097.280 | 300 | 30 | 0.2 | 24.822 | 0.711 | 0.289 |
2 | 6.096 | 1103.376 | 300 | 30 | 0.2 | 24.877 | 0.652 | 0.348 |
3 | 6.096 | 1109.472 | 300 | 30 | 0.2 | 24.932 | 0.527 | 0.473 |
4 | 6.096 | 1115.568 | 300 | 30 | 0.2 | 24.981 | 0.351 | 0.649 |
5 | 9.144 | 1123.188 | 300 | 30 | 0.2 | 25.050 | 0.131 | 0.869 |
6 (bottom) | 15.240 | 1135.380 | 300 | 30 | 0.2 | 25.167 | 0.000 | 1.000 |
Parameters | Value |
---|---|
Stock tank oil density, g/cm3 | 0.721 |
Initial oil viscosity, mPa∙s | 0.95 |
Oil compressibility, MPa−1 | 1.45 × 10−3 |
Oil formation volume factor | 1.11 |
Initial water density, g/cm3 | 0.995 |
Initial water viscosity, mPa∙s | 0.96 |
Water compressibility, MPa−1 | 4.35 × 10−4 |
Water formation volume factor | 1.014 |
Rock compressibility, MPa−1 | 5.80 × 10−4 |
Bottom hole pressure of injection well, MPa | 25.512 |
Minimum bottom hole pressure of production well, MPa | 10.343 |
Liquid rate of production well, m3/d | 477 |
0.2200 | 0.0000 | 1.0000 | 0.0434 |
0.3000 | 0.0700 | 0.4000 | 0.0248 |
0.4000 | 0.1500 | 0.1250 | 0.0186 |
0.5000 | 0.2400 | 0.0649 | 0.0155 |
0.6000 | 0.3300 | 0.0048 | 0.0124 |
0.8000 | 0.6500 | 0.0000 | 0.0062 |
0.9000 | 0.8300 | 0.0000 | 0.0031 |
1.0000 | 1.0000 | 0.0000 | 0.0000 |
Parameters of the Heavy Oil Displacement Experiment | Value | Input Parameters of the Designed Simulator | Value |
---|---|---|---|
Temperature, °C | 65 | Number of blocks along x | 59 |
Oil sample number | #1 | Number of blocks along y | 5 |
Core dimensions, cm | 29.5 × 4.5 × 4.5 | Number of blocks along z | 5 |
Porosity, fraction | 0.246 | Length of the block along x, cm | 0.5 |
Permeability, mD | 1200 | Length of the block along y, cm | 0.9 |
Rock compressibility, MPa−1 | 2.6 × 10−4 | Length of the block along z, cm | 0.9 |
Stock tank oil density, g/cm3 | 0.956 | Initial porosity, fraction | 0.246 |
Oil viscosity, mPa∙s | 180 | Initial permeability in x direction, mD | 1200 |
Oil compressibility, MPa−1 | 1.0 × 10−3 | Initial permeability in y direction, mD | 1200 |
Oil formation volume factor | 1.066 | Initial permeability in z direction, mD | 120 |
Water density, g/cm3 | 1 | Rock compressibility, MPa−1 | 2.6 × 10−4 |
Water viscosity, mPa∙s | 0.52 | Stock tank oil density, g/cm3 | 0.956 |
Water compressibility, MPa−1 | 4.6 × 10−4 | Initial oil viscosity, mPa∙s | 180 |
Water formation volume factor | 1.012 | Oil compressibility, MPa−1 | 1.0 × 10−3 |
Initial pressure, MPa | 2 | Oil formation volume factor | 1.066 |
Water saturation, fraction | 0.272 | Initial water density, g/cm3 | 1 |
Oil saturation, fraction | 0.728 | Water viscosity, mPa∙s | 0.52 |
Bottom hole pressure of production well, MPa | 2 | Water compressibility, MPa−1 | 4.6 × 10−4 |
Water rate of injection well, cm3/min | 0.5 | Water formation volume factor | 1.012 |
TPG, MPa/m | 0.0005 | Initial pressure, MPa | 2 |
initial water saturation, fraction | 0.272 | ||
initial oil saturation, fraction | 0.728 | ||
Bottom hole pressure of production well, MPa | 2 | ||
Water rate of injection well, cm3 min−1 | 0.5 | ||
TPG, MPa/m | 0.0005 |
, MPa | |||
---|---|---|---|
0.2720 | 0.0000 | 1.0000 | 0.1674 |
0.3014 | 0.0024 | 0.8531 | 0.1473 |
0.3308 | 0.0039 | 0.7156 | 0.1268 |
0.3602 | 0.0051 | 0.5877 | 0.1088 |
0.3896 | 0.0071 | 0.4692 | 0.0962 |
0.4190 | 0.0098 | 0.3578 | 0.0830 |
0.4484 | 0.0142 | 0.2583 | 0.0727 |
0.4778 | 0.0257 | 0.1659 | 0.0629 |
0.5072 | 0.0488 | 0.0723 | 0.0549 |
0.5366 | 0.0829 | 0.0213 | 0.0477 |
0.5660 | 0.1209 | 0.0118 | 0.0420 |
0.5954 | 0.1588 | 0.0088 | 0.0362 |
0.6248 | 0.1943 | 0.0071 | 0.0307 |
0.6542 | 0.2299 | 0.0061 | 0.0261 |
0.6836 | 0.2654 | 0.0052 | 0.0186 |
0.7130 | 0.3033 | 0.0038 | 0.0113 |
0.7424 | 0.3452 | 0.0012 | 0.0043 |
0.7718 | 0.3886 | 0.0000 | 0.0000 |
Parameters | Simulation Number | ||||
---|---|---|---|---|---|
#1 | #2 | #3 | #4 | #5 | |
Number of blocks along x | 15 | 31 | 59 | 71 | 81 |
Number of blocks along y | 3 | 3 | 5 | 7 | 9 |
Number of blocks along z | 3 | 3 | 5 | 7 | 9 |
Length of the block along x, cm | 1.9667 | 0.9516 | 0.5 | 0.4155 | 0.3642 |
Length of the block along y, cm | 1.5 | 1.5 | 0.9 | 0.6429 | 0.5 |
Length of the block along z, cm | 1.5 | 1.5 | 0.9 | 0.6429 | 0.5 |
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Xin, X.; Li, Y.; Yu, G.; Wang, W.; Zhang, Z.; Zhang, M.; Ke, W.; Kong, D.; Wu, K.; Chen, Z. Non-Newtonian Flow Characteristics of Heavy Oil in the Bohai Bay Oilfield: Experimental and Simulation Studies. Energies 2017, 10, 1698. https://doi.org/10.3390/en10111698
Xin X, Li Y, Yu G, Wang W, Zhang Z, Zhang M, Ke W, Kong D, Wu K, Chen Z. Non-Newtonian Flow Characteristics of Heavy Oil in the Bohai Bay Oilfield: Experimental and Simulation Studies. Energies. 2017; 10(11):1698. https://doi.org/10.3390/en10111698
Chicago/Turabian StyleXin, Xiankang, Yiqiang Li, Gaoming Yu, Weiying Wang, Zhongzhi Zhang, Maolin Zhang, Wenli Ke, Debin Kong, Keliu Wu, and Zhangxin Chen. 2017. "Non-Newtonian Flow Characteristics of Heavy Oil in the Bohai Bay Oilfield: Experimental and Simulation Studies" Energies 10, no. 11: 1698. https://doi.org/10.3390/en10111698
APA StyleXin, X., Li, Y., Yu, G., Wang, W., Zhang, Z., Zhang, M., Ke, W., Kong, D., Wu, K., & Chen, Z. (2017). Non-Newtonian Flow Characteristics of Heavy Oil in the Bohai Bay Oilfield: Experimental and Simulation Studies. Energies, 10(11), 1698. https://doi.org/10.3390/en10111698