N-(diisopropylphosphanyl)benzamide
Round 1
Reviewer 1 Report
The manuscript molbank-2449487 "N-(diisopropylphosphanyl)benzamide" by Peloso and co-workers is describes the synthesis of N-(diisopropylphosphanyl)benzamide via two synthetic routes. The synthesis was confirmed by 1H, 13C NMR, IR spectroscopy and single crystal X-ray diffraction analyses. I think this paper will be of interest to the readers of Molbank.
However, I have some recommendations:
1) Please add the compounds yield under the structures in Scheme 1.
2) Please add the IR spectrum image of compound 1 in the Supplementary materilas/
3) Since compound 1 was synthesized for the first time, I recommend registering the mass spectrum.
Author Response
We kindly thank the reviewer for comments and suggestions.
1) Yields have been added;
2) the FT-IR spectrum of 1 has been included in the SI.
3) Unfortunately, we will not be able to register the mass spectrum of 1 over the next months.
