8-(Pyrimidin-2-yl)-1,2,3,4,5,6,7,8-heptathiazocane
1
N. D. Zelinsky Institute of Organic Chemistry Russian Academy of Sciences, 47 Leninsky Prospekt, Moscow 119991, Russia
2
Nanotechnology Education and Research Center, South Ural State University, 76 Lenina Avenue, Chelyabinsk 454080, Russia
*
Author to whom correspondence should be addressed.
Molbank 2019, 2019(4), M1091; https://doi.org/10.3390/M1091
Received: 29 October 2019 / Revised: 18 November 2019 / Accepted: 18 November 2019 / Published: 20 November 2019
(This article belongs to the Section Organic Synthesis)
Heptasulfur imides substituted by hereterocycle may be of interest as biologically active compounds. In this communication, the reaction of pyrimidin-2-amine 1 with disulfur dichloride was carefully investigated to give 8-(pyrimidin-2-yl)-1,2,3,4,5,6,7,8-heptathiazocane in good yield. The structure of the newly synthesized compound was established by means of elemental analysis, high resolution mass-spectrometry, 1H, 13C NMR and IR spectroscopy and mass-spectrometry.
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Keywords:
heptasulfur imides; pyrimidin-2-amine; disulfur dichloride
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MDPI and ACS Style
Ogurtsov, V.A.; Rakitin, O.A. 8-(Pyrimidin-2-yl)-1,2,3,4,5,6,7,8-heptathiazocane. Molbank 2019, 2019, M1091. https://doi.org/10.3390/M1091
AMA Style
Ogurtsov VA, Rakitin OA. 8-(Pyrimidin-2-yl)-1,2,3,4,5,6,7,8-heptathiazocane. Molbank. 2019; 2019(4):M1091. https://doi.org/10.3390/M1091
Chicago/Turabian StyleOgurtsov, Vladimir A.; Rakitin, Oleg A. 2019. "8-(Pyrimidin-2-yl)-1,2,3,4,5,6,7,8-heptathiazocane" Molbank 2019, no. 4: M1091. https://doi.org/10.3390/M1091
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