Synthesis and Characterization of Dimethacrylate Monomer with High Molecular Weight for Root Canal Filling Materials
1
College of Materials Science and Engineering, South China University of Technology, Guangzhou 510641, China
2
Guanghua College of Stomatology, Institute of Stomatology, Sun Yat-sen University, Guangzhou 510060, China
*
Author to whom correspondence should be addressed.
Molecules 2006, 11(12), 953-958; https://doi.org/10.3390/11120953
Received: 18 November 2006 / Revised: 4 December 2006 / Accepted: 4 December 2006 / Published: 7 December 2006
A new dimethacrylate monomer 9,9'-bis[4-(2'-hydroxy-3'-methacryloyloxy-propoxy)phenyl] fluorene (3) with a molecular weight of 634 was synthesized in 51.4%yield by addition of a glycidyl ether group to 9,9'-bis(4-hydroxyphenyl) fluorene (1) bythe reaction of compound 1 with epichlorohydrin, and then introducing the methacrylatemoiety by the reaction of the epoxy group with methacrylic acid. The structure ofmonomer 3 was confirmed by FT-IR, 1H-NMR, mass spectra and elemental analysis.
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Keywords:
Dimethacrylates; high molecular weight; synthesis; characterization.
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MDPI and ACS Style
Liu, F.; He, J.-W.; Lin, Z.-M.; Ling, J.-Q.; Jia, D.-M. Synthesis and Characterization of Dimethacrylate Monomer with High Molecular Weight for Root Canal Filling Materials. Molecules 2006, 11, 953-958.
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