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Keywords = tetrahydrophenocucurbituril

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12 pages, 809 KiB  
Article
Microwave Synthesis of Au Nanoparticles in the Presence of Tetrahydrothiophenocucurbituril
by Asma S. Atthar, Shreya Saha, Ahmed Abdulrahman and Anthony I. Day
Molecules 2024, 29(1), 168; https://doi.org/10.3390/molecules29010168 - 27 Dec 2023
Cited by 2 | Viewed by 1316
Abstract
The preparation of gold nanoparticles (AuNPs) from tetrachloroauric acid in the presence of tetrahydrothiophenocucurbit[n]uril (THTmQ[n]) has been effectively achieved in a microwave reactor. The reaction was performed in the presence of an excess of the tetrahydrothiopheno function [...] Read more.
The preparation of gold nanoparticles (AuNPs) from tetrachloroauric acid in the presence of tetrahydrothiophenocucurbit[n]uril (THTmQ[n]) has been effectively achieved in a microwave reactor. The reaction was performed in the presence of an excess of the tetrahydrothiopheno function in a partial reductant role, while the remainder formed AuNP-THTmQ[n] conjugates after the reduction was completed with formic acid. An affinity for the AuNPs by the THTmQ[n] was observed in the purification of the NPs via centrifugation, removal of the supernatant and resuspension of the conjugate. Full article
(This article belongs to the Section Nanochemistry)
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