Search Results (6)

Fibrous materials are often used in the manufacturing of fire protection devices such as fire curtains. Their optimization and improved performance is still a topic of interest. The present work aims to develop and test a new combination of fibers arranged in various 2D and 3D patterns with coatings. For this purpose, basalt fibers were added into a glass fiber fabric, and wires of a shape memory material (SMM) were inserted into the fabric to create air pockets induced by temperature. In fire curtains, the base structure is a 2D basket pattern, and all combinations were tested with and without a waterborne polyurethane (WPU) coating with inorganic materials. Three different tests were selected to characterize the thermal behavior: fire resistance, ignitability, and smoke production. Fiberglass proved to be the best material to provide thermal resistance in fire curtains, with the outer surface temperature of the fabric below 650 °C at the end of the tests. The SMM wires provided good protection during the initial stages of the test, but a combination of excessive deformation and reduced strength of the fabric resulted in a sudden failure of the structure. Basalt fibers contribute to a reduction of smoke production. It was observed an improvement of up to 10% in the thermal capacity between 1MIX2 (glass fibers fabric with coating, MIX2) and the best commercial curtain evaluated, Commercial3 (glass and steel fibers fabric with coating). Full article

Epitaxially regrown electrically pumped photonic crystal surface emitting lasers (PCSELs) operating near 2 µm were designed and fabricated within a III-V-Sb material system. A high-index-contrast photonic crystal layer was incorporated into the laser heterostructures by air-pocket-retaining epitaxial regrowth. Transmission electron microscopy studies confirmed uniform and continuous AlGaAsSb initial growth over the nano-patterned GaSb surface, followed by the development of the air-pockets. The PCSEL threshold current density had a minimal value of ~170 A/cm² in the 160–180 K temperature range when the QW gain spectrum aligned with the Γ₂ band edge of the photonic crystal. The devices operated in a continuous wave regime at 160 K. The divergence and polarization of the multimode laser beam emitted from the 200 µm × 200 µm PCSEL aperture were controlled by filamentation. Full article

A simple and hands-on one-step process has been implemented to fabricate polymer-templated hydrophobic nanostructures as hydrogen gas sensing platforms. Topographic measurements have confirmed irregular hills and dips of various dimensions that are responsible for creating air bubble pockets that satisfy the Cassie–Baxter state of hydrophobicity. High-resolution field-emission scanning electron microscopy (FESEM) has revealed double-layer structures consisting of fine microscopic flower-like structures of nanoscale petals on the top of base nanostructures. Wetting contact angle (WCA) measurements further revealed the contact angle to be ~142.0° ± 10.0°. Such hydrophobic nanostructures were expected to provide a platform for gas-sensing materials of a higher surface area. From this direction, a very thin layer of palladium, ca. 100 nm of thickness, was sputtered. Thereafter, further topographic and WCA measurements were carried out. FESEM micrographs revealed that microscopic flower-like structures of nanoscale petals remained intact. A sessile drop test reconfirmed a WCA of as high as ~130.0° ± 10.0°. Due to the inherent features of hydrophobic nanostructures, a wider surface area was expected that can be useful for higher target gas adsorption sites. In this context, a customized sensing facility was set up, and H₂ gas sensing performance was carried out. The surface nanostructures were found to be very stable and durable over the course of a year and beyond. A polymer-based hydrophobic gas-sensing platform as investigated in this study will play a dual role in hydrophobicity as well as superior gas-sensing characteristics. Full article

Polymer-based micro-electrode arrays (MEAs) are gaining attention as an essential technology to understand brain connectivity and function in the field of neuroscience. However, polymer based MEAs may have several challenges such as difficulty in performing the etching process, difficulty of micro-pattern generation through the photolithography process, weak metal adhesion due to low surface energy, and air pocket entrapment over the electrode site. In order to compensate for the challenges, this paper proposes a novel MEA fabrication process that is performed sequentially with (1) silicon mold preparation; (2) PDMS replica molding, and (3) metal patterning and parylene insulation. The MEA fabricated through this process possesses four arms with electrode sites on the convex microstructures protruding about 20 μm from the outermost layer surface. The validity of the convex microstructure implementation is demonstrated through theoretical background. The electrochemical impedance magnitude is 204.4 ± 68.1 kΩ at 1 kHz. The feasibility of the MEA with convex microstructures was confirmed by identifying the oscillation in the beta frequency band (13–30 Hz) in the electrocorticography signal of a rat olfactory bulb during respiration. These results suggest that the MEA with convex microstructures is promising for applying to various neural recording and stimulation studies. Full article

Harnesses can be used in various applications, such as entertainment, rescue operations, and medical applications. Because users are supported on the harness for a long time, they should feel comfortable wearing the harnesses. However, existing commercial harnesses are uncomfortable to wear and cause continuous serious pain. Therefore, in this study, a new pant-type harness with a fabric air pocket to reduce the applied pressure on the body, especially in the groin, is proposed. Keeping this in mind, we have designed and developed the pant-type harness. In addition, we performed pressure and contact area measurement experiments using the harness developed, pressure sensor, and a human mannequin. Peak and mean pressures and contact areas near the groin and waist were measured in the experiments. From the results, when air is injected in the air pockets, the peak pressure and contact area near the waist increased, and the peak pressure near the groin decreased. This means that the pressure applied on the human mannequin near the groin reduces because of the increased contact area near the waist, which is achieved by multi-layered air pockets. In this study, we proposed the optimal design of a novel pant-type harness that can address the limitations of existing harnesses. The proposed harness can be used for a prolonged time in applications, such as virtual reality entertainment, rescue operations, and rehabilitation. Full article

Liquid marbles are versatile structures demonstrating a pseudo-Leidenfrost wetting regime formed by encapsulating microscale volumes of liquid in a particle shell. The liquid core is completely separated from the exterior through air pockets. The external phase consists of hydrophobic particles, in most cases, or hydrophilic ones distributed as aggregates. Their interesting features arise from the double solid-fluid character. Thus, these interesting formations, also known as “dry waters”, have gained attention in surface science. This review paper summarizes a series of proposed formulations, fabrication techniques and properties, in correlation with already discovered and emerging applications. A short general review of the surface properties of powders (contact angle, superficial tension) is proposed, followed by a presentation of liquid marbles’ properties (superficial characteristics, elasticity, self-propulsion etc.). Finally, applications of liquid marbles are discussed, mainly as helpful and yet to be exploited structures in the pharmaceutical and medical field. Innovative pharmaceutical forms (Pickering emulsions) are also means of use taken into account as applications which need further investigation. Full article