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Keywords = cobaltosic oxide

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14 pages, 14207 KiB  
Article
Synthesis of Needle-like Nanostructure Composite Electrode of Co3O4/rGO/NF for High-Performance Symmetric Supercapacitor
by Xiaoyan Wang, Shixiang Lu and Wenguo Xu
Crystals 2022, 12(5), 664; https://doi.org/10.3390/cryst12050664 - 5 May 2022
Cited by 22 | Viewed by 3667
Abstract
In this work, a hierarchical electrode structure of cobaltosic oxide (Co3O4) growing on a reduced graphene oxide (rGO)-covered nickel foam (NF) substrate (named Co3O4/rGO/NF) is fabricated by a facile hydrothermal and subsequent annealing process. Thousands [...] Read more.
In this work, a hierarchical electrode structure of cobaltosic oxide (Co3O4) growing on a reduced graphene oxide (rGO)-covered nickel foam (NF) substrate (named Co3O4/rGO/NF) is fabricated by a facile hydrothermal and subsequent annealing process. Thousands of nanoneedle units uniformly arranged on the surface of the rGO sheet stimulate the evident increase in the specific surface area and thus produce more active sites. Because of the special hierarchical structure, the Co3O4/rGO/NF electrode shows a high specific capacitance of 1400 F g−1 at 1 A g−1 and retains 58% capacitance even when the current density increases to 30 A g−1. In addition, a symmetric supercapacitor based on the Co3O4/rGO/NF electrode is assembled, exhibiting high specific capacitance of 311 F g−1 at 1 A g−1, as well as remarkable power density and energy density (40.67 Wh kg−1 at 12 kW kg−1). The device also demonstrates a great cycling performance after 10,000 cycles under the current density of 10 A g−1, acquiring 89.69% capacitance retention of the initial state. The accessible synthetic method and superior electrochemical performance of the Co3O4/rGO/NF composite electrode implicate its extensive application prospects in terms of new energy storage. Full article
(This article belongs to the Special Issue Supercapacitors with High Energy Density)
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16 pages, 3436 KiB  
Article
Effect of Fluoride on the Morphology and Electrochemical Property of Co3O4 Nanostructures for Hydrazine Detection
by Tuantuan Zhou, Wanlin Gao, Qiang Wang and Ahmad Umar
Materials 2018, 11(2), 207; https://doi.org/10.3390/ma11020207 - 29 Jan 2018
Cited by 28 | Viewed by 5164
Abstract
In this paper, we systematically investigated the influence of fluoride on the morphology and electrochemical property of Co3O4 nanostructures for hydrazine detection. The results showed that with the introduction of NH4F during the synthesis process of Co3 [...] Read more.
In this paper, we systematically investigated the influence of fluoride on the morphology and electrochemical property of Co3O4 nanostructures for hydrazine detection. The results showed that with the introduction of NH4F during the synthesis process of Co3O4, both Co(CO3)0.5(OH)·0.11H2O and Co(OH)F precursors would be generated. To understand the influence of F on the morphology and electrochemical property of Co3O4, three Co3O4 nanostructures that were respectively obtained from bare Co(CO3)0.5(OH)·0.11H2O, Co(OH)F and Co(CO3)0.5(OH)·0.11H2O mixtures and bare Co(OH)F were successfully synthesized. The electrochemical tests revealed the sensing performance of prepared Co3O4 nanostructures decreased with the increase in the fluoride contents of precursors. The more that dosages of NH4F were used, the higher crystallinity and smaller specific surface area of Co3O4 was gained. Among these three Co3O4 nanostructures, the Co3O4 that was obtained from bare Co(CO3)0.5(OH)·0.11H2O-based hydrazine sensor displayed the best performances, which exhibited a great sensitivity (32.42 μA·mM−1), a low detection limit (9.7 μΜ), and a wide linear range (0.010–2.380 mM), together with good selectivity, great reproducibility and longtime stability. To the best of our knowledge, it was revealed for the first time that the sensing performance of prepared Co3O4 nanostructures decreased with the increase in fluoride contents of precursors. Full article
(This article belongs to the Special Issue Advanced Functional Nanomaterials and Their Applications)
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