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Authors = Katarzyna Wolowik

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5 pages, 174 KiB  
Article
Microwave-Accelerated or Conventionally Heated Iodination Reactions of Some Aromatic Amines, Using ortho-Periodic Acid as the Oxidant †
by Maciej Sosnowski, Lech Skulski and Katarzyna Wolowik
Molecules 2004, 9(7), 617-621; https://doi.org/10.3390/90700617 - 30 Jun 2004
Cited by 11 | Viewed by 7171
Abstract
A fast and simple method for the oxidative iodination of some aromatic amines, either under microwave irradiation or conventional heating, is reported, using diiodine and ortho-periodic acid as the oxidant. The reactions were carried out in boiling CH2Cl2 solutions under a reflux condenser. [...] Read more.
A fast and simple method for the oxidative iodination of some aromatic amines, either under microwave irradiation or conventional heating, is reported, using diiodine and ortho-periodic acid as the oxidant. The reactions were carried out in boiling CH2Cl2 solutions under a reflux condenser. For the microwave assisted reactions, the reaction times were always notably shortened, but the yields were usually less influenced as compared with the conventional method. Full article
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