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1 Citations

1,959 Views

14 Pages

Non-Selective Reduction of P-Stereogenic Phosphinoylacetic Acid Esters and 3-Phosphorylated Coumarins to Phosphino-Boranes: Discovery of Unexpected 2,3-Dihydrobenzofuran Derivative

Kamil Dziuba,
Natalia Walczak and
Katarzyna Szwaczko

Symmetry2024, 16(8), 976;https://doi.org/10.3390/sym16080976

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1 August 2024

This paper presents the efficient reduction of phosphinoylacetic acid esters and 3-phosphorylated coumarin to their corresponding phosphino-boranes using BH₃-THF complexes. Optimized conditions for the reduction of phosphinoylacetic acid esters...

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Article

2 Citations

2,287 Views

15 Pages

Mono-Alkyl-Substituted Phosphinoboranes (HRP–BH₂–NMe₃) as Precursors for Poly(alkylphosphinoborane)s: Improved Synthesis and Comparative Study

Felix Lehnfeld,
Tim Oswald,
Rüdiger Beckhaus and
Manfred Scheer

Inorganics2023, 11(10), 377;https://doi.org/10.3390/inorganics11100377

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23 September 2023

A new synthetic pathway to various mono-alkyl-substituted phosphinoboranes HRP–BH₂–NMe₃ has been developed. The new synthetic route starting from alkyl halides and NaPH₂ followed by metalation and salt metathesis is performed in a one-pot...

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2 Results Found

Non-Selective Reduction of P-Stereogenic Phosphinoylacetic Acid Esters and 3-Phosphorylated Coumarins to Phosphino-Boranes: Discovery of Unexpected 2,3-Dihydrobenzofuran Derivative

Mono-Alkyl-Substituted Phosphinoboranes (HRP–BH2–NMe3) as Precursors for Poly(alkylphosphinoborane)s: Improved Synthesis and Comparative Study

Mono-Alkyl-Substituted Phosphinoboranes (HRP–BH₂–NMe₃) as Precursors for Poly(alkylphosphinoborane)s: Improved Synthesis and Comparative Study