Search Results (3)

The detection of three-dimensional displacement, caused by micro-nano scale deformation, is of great significance for the industrial production of glass or quartz optical fiber products. Considering the detection cost and practicability, an image spherizing-based three-dimensional displacement measurement method for a monocular microscopic imaging system (a microscope with a normal industrial camera) is proposed. Differential theory tells us that an arbitrary large-scale deformation can be approximatively considered as the sum of slope-shaped deformations. In this paper, an ordinary slope model is presented by the idea of image spherizing and differential theory, which reveals the mathematical relation between in-plane displacement and out-of-plane displacement in the deformed images captured by an optical microscope. After obtaining the in-plane displacement field, the out-of-plane displacement field can be extracted from the in-plane displacement field by the ordinary slope model, which indicates that the out-of-plane displacement information carried by the in-plane displacement is fully utilized. Simulation and application experiments are performed to demonstrate the effectiveness and all the absolute errors of the measurement by optical microscope with a magnification of 50× are less than 0.2 μm. Unlike conventional methods, the new method does not need a phase unwrapping process during detection and has many attractive characteristics such as low-cost, simple arrangements and good applicability. Because the measurement precision of this technique can meet the detection requirement, it has been applied to the industrial detection of glass or quartz optical fiber products. Full article

Due to the monitoring requirement of optical fiber industrial production, an out-of-plane displacement measurement method is proposed. Firstly, the in-plane displacements between two consecutive images, captured through a microscope with a CCD camera, are estimated by the Digital Speckle Correlation Method (DSCM). Subsequently, the out-of-plane displacement of optical fiber material can be obtained by the wedge model. Finally, the effectiveness of the method is verified experimentally by comparing the measurement data of routine practice with its theoretical values. Simulation and experimental results indicate that the absolute errors and the relative errors of the measurement by the optical microscope with a magnification of 50× are less than ±0.2 μm and 5%, respectively. The new method only needs two images obtained by the microscopic imaging system with a single camera to accomplish the measurement, which can significantly reduce the measurement time and complexity of the arrangement. Further, the method needs neither frequency domain conversion nor phase unwrapping operation, therefore, it is especially suitable for dynamic out-of-plane displacement measurement. The proposed method has been applied to the industrial uniformity and micro–nano-scale deformation monitoring of optical fiber image transmission materials. Full article

The spherization of nanoenergetic materials is the best way to improve the sensitivity and increase loading densities and detonation properties for weapons and ammunition, but the preparation of spherical nanoenergetic materials with high regularization, uniform size and monodispersity is still a challenge. In this paper, nanoenergetic hollow spherical hexanitrostibene (HNS) derivatives were fabricated via a one-pot copolymerization strategy, which is based on the reaction of HNS and piperazine in acetonitrile solution. Characterization results indicated the as-prepared reaction nanoenergetic products were HNS-derived oligomers, where a free radical copolymerization reaction process was inferred. The hollow sphere structure of the HNS derivatives was characterized by scanning electron microscopy (SEM), transmission electron microscope (TEM), and synchrotron radiation X-ray imaging technology. The properties of the nanoenergetic hollow spherical derivatives, including thermal decomposition and sensitivity are discussed in detail. Sensitivity studies showed that the nanoenergetic derivatives exhibited lower impact, friction and spark sensitivity than raw HNS. Thermogravimetric-differential scanning calorimeter (TG-DSC) results showed that continuous exothermic decomposition occurred in the whole temperature range, which indicated that nanoenergetic derivatives have a unique role in thermal applications. Therefore, nanoenergetic hollow spherical HNS derivatives could provide a new way to modify the properties of certain energetic compounds and fabricate spherical nanomaterials to improve the charge configuration. Full article