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Table of Contents

Molecules, Volume 6, Issue 10 (October 2001), Pages 796-844

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	p. 796-802 Wolfgang Holzer Article: Unambiguous Assignment of the 1H- and 13C-NMR Spectra of Propafenone and a Thiophene Analogue Molecules 2001, 6(10), 796-802; doi:10.3390/61000796 Received: 4 December 2000; in revised form: 12 September 2001 / Accepted: 12 September 2001 / Published: 30 September 2001 Show/Hide Abstract | Download PDF Full-text (38 KB) Abstract: Full and unambiguous asssignment of all 1H- and 13C-NMR resonances of the free bases as well as the hydrochloride salts of the antiarrhythmic agent propafenone and a thiophene analogue in different solutions (DMSO-d6, CDCl3) is reported.
	p. 803-814 Fatiha Belferdi and Abdelhamid Belattar Article: Synthesis of the Aspidosperma Alkaloid Na-Formyl-16-α-Hydroxyaspidospermidine Molecules 2001, 6(10), 803-814; doi:10.3390/61000803 Received: 1 April 2001; in revised form: 6 September 2001 / Accepted: 8 September 2001 / Published: 30 September 2001 Show/Hide Abstract | Download PDF Full-text (110 KB) Abstract: The first total synthesis of Na-formyl-16α-hydroxyaspidospermidine and its isomer via (±)-vincadifformine is described and their structure elucidation using different methods of analysis is reported.
	p. 815-824 Katica Colanceska-Ragenovic, Vesna Dimova, Vlado Kakurinov, Dora Gabor Molnar and Aleksandra Buzarovska Article: Synthesis, Antibacterial and Antifungal Activity of 4-Substituted-5-Aryl-1,2,4-Triazoles Molecules 2001, 6(10), 815-824; doi:10.3390/61000815 Received: 8 February 2001; in revised form: 24 September 2001 / Accepted: 26 September 2001 / Published: 30 September 2001 Show/Hide Abstract | Download PDF Full-text (93 KB) Abstract: A few 4-allyl/amino-5-aryl-1,2,4-triazoles were synthesized and tested for antibacterial and antifungal effects against Escherichia coli, Bacillus subtilis, Salmonella enteritidis, Staphylococcus aureus, Aspergillus niger and Candida albicans. 4-Allyl-5-aryl-1,2,4-triazoles were obtained by the oxidative cyclization of the appropriate 1-substituted-4-allylthiosemicarbazides and 4-amino-5-aryl-1,2,4-triazoles were obtained by cyclization of the potassium salts of appropriately substituted dithiocarbazinic acids with hydrazine hydrate. The new synthesized compounds were characterized using IR, 1H- NMR, 13C-NMR and UV spectral data together with elemental analysis.
	p. 825-830 Franz Müller and John Lee Article: A Convenient Method to Prepare Labile FMN Derivatives Molecules 2001, 6(10), 825-830; doi:10.3390/61000825 Received: 30 September 2001 / Accepted: 10 October 2001 / Published: 31 October 2001 Show/Hide Abstract | Download PDF Full-text (30 KB) Abstract: A simple method for selective phosphorylation of ribityl containing starting materials to afford FMN derivatives is presented. The method is in particular valuable for the synthesis of labile FMN derivatives.
	p. 831-844 Didier Villemin, Mohamed Hammadi, Messaoud Hachemi and Nathalie Bar Article: Applications of Microwave in Organic Synthesis: An Improved One-step Synthesis of Metallophthalocyanines and a New Modified Microwave Oven for Dry Reactions Molecules 2001, 6(10), 831-844; doi:10.3390/61000831 Received: 7 September 2001 / Accepted: 10 October 2001 / Published: 31 October 2001 Show/Hide Abstract | Download PDF Full-text (101 KB) Abstract: Metallophthalocyanine complexes are obtained quickly and efficiently by the reaction of phthalodinitrile with hydrated metallic salts without solvent and under microwave irradiation. The use of a modified commercial microwave oven to perform this type of reactions under dry conditions is described. Metallophthalocyanines and metallododecachlorophthalocyanines of some divalent metals can be also obtained from phthalic or tetrachlorophthalic anhydrides with hydrated metallic salt and urea under microwave irradiation and without solvent.
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