Next Article in Journal
Effect of Extraction Solvent/Technique on the Antioxidant Activity of Selected Medicinal Plant Extracts
Next Article in Special Issue
Efficient Microwave Assisted Syntheses of 2,5-Diketopiperazines in Aqueous Media
Previous Article in Journal
Cyclization of Hydrazones of 2-Acetyl-1-naphthol and 1-Acetyl-2-naphthol with Triphosgene. Synthesis of Spiro Naphthoxazine Dimers
Previous Article in Special Issue
Synthesis of γ-Nitro Aliphatic Methyl Esters Via Michael Additions Promoted by Microwave Irradiation
Article Menu

Export Article

Open AccessArticle
Molecules 2009, 14(6), 2160-2166; https://doi.org/10.3390/molecules14062160

Extraction with SPME and Synthesis of 2-Methyl-6-vinylpyrazine by a ‘One Pot’ Reaction Using Microwaves

1
Centro de Desarrollo de Productos Bióticos, IPN. Km. 8.5 Carretera Yautepec-Jojutla Yautepec, Morelos, C.P. 62731, Mexico
2
Centro de Investigaciones Químicas, Universidad Autónoma del Estado de Morelos. Av. Universidad No. 1001, Col. Chamilpa, C.P. 62210 Cuernavaca, Mor., Mexico
*
Author to whom correspondence should be addressed.
Received: 20 April 2009 / Revised: 30 May 2009 / Accepted: 2 June 2009 / Published: 15 June 2009
(This article belongs to the Special Issue Microwave Assisted Synthesis)
View Full-Text   |   Download PDF [224 KB, uploaded 18 June 2014]   |  

Abstract

A synthesis of 2-methyl-6-vinylpyrazine was carried out by way of a ‘one pot’ reaction. In order to establish the efficiency of this synthesis the extraction of the volatiles released by male papaya fruit flies was performed by SPME (solid phase micro-extraction). The compound was separated and identified using GC/MSD (gas chromatography/mass spectrometry detector). View Full-Text
Keywords: SPME; Hoffman methylation; microwave; 2-methyl-6-vinylpyrazine; sexual pheromone SPME; Hoffman methylation; microwave; 2-methyl-6-vinylpyrazine; sexual pheromone
Figures

Graphical abstract

This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

Share & Cite This Article

MDPI and ACS Style

Robledo, N.; Escalante, J.; Arzuffi, R. Extraction with SPME and Synthesis of 2-Methyl-6-vinylpyrazine by a ‘One Pot’ Reaction Using Microwaves. Molecules 2009, 14, 2160-2166.

Show more citation formats Show less citations formats

Related Articles

Article Metrics

Article Access Statistics

1

Comments

[Return to top]
Molecules EISSN 1420-3049 Published by MDPI AG, Basel, Switzerland RSS E-Mail Table of Contents Alert
Back to Top