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Int. J. Mol. Sci. 2008, 9(6), 1000-1007; doi:10.3390/ijms9061000

Synthesis and Characterization of Some New Tetraaldehyde and Tetraketone Derivatives and X-ray Structure of 1,1'-(4,4'-(2- (1,3-bis(4-Acetylphenoxy)propan-2-ylidene)propane-1,3-diyl) bis(oxy)bis(4,1-phenylene))diethanone

1
Department of Chemistry Faculty of Arts and Sciences Karadeniz Teknik University, 61080-Trabzon, Turkey
2
Department of Middle Education, Educational Faculty, Ondokuz Mayıs University 55200-Atakum-Samsun, Turkey
3
Department of Computer Education and Instructional Technology, Educational Faculty, Ondokuz Mayıs University 55200-Atakum-Samsun, Turkey
4
Departamento de Química Inorgánica, Facultade de Ciencias-Química, Universidade de Vigo, 36200-Vigo, Galicia, Spain
*
Author to whom correspondence should be addressed.
Received: 26 November 2007 / Revised: 15 April 2008 / Accepted: 18 April 2008 / Published: 13 June 2008
(This article belongs to the Section Physical Chemistry, Theoretical and Computational Chemistry)
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Abstract

Tetraketone and tetraaldehyde derivatives 2a-d were synthesized via the reaction of ethene-1,1,2,2,-tetra-yl-tetramethylene tetrabromide (1) with hydroxyketone and aldehyde derivatives. The molecular structures were identifed by IR, 1H-NMR, 13CNMR and MS analysis. The crystal structure of the title compound 2a, C38H36O8, is reported. Its crystal data are: monoclinic, space group P 2(1)/n with cell dimensions of a= 9.0395(12) Å ,b= 12.6114(17) Å, c = 13.8166(18) Å, β= 95.875(3), V= 1566.8(4) Å3, F.W.= 620.67, ρcalc =1.316 gcm3 for Z=2, μ=0.092 mm-1
Keywords: 1; 3-bis(4-Acetylphenoxy)propan-2-ylidenepropane; 1; 3-di-ylbis(oxy)bis(4; 1- phenylene))diethanone; crystal structure; x-ray 1; 3-bis(4-Acetylphenoxy)propan-2-ylidenepropane; 1; 3-di-ylbis(oxy)bis(4; 1- phenylene))diethanone; crystal structure; x-ray
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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MDPI and ACS Style

Er, M.; Ustabaş, R.; Çoruh, U.; Sancak, K.; Vázquez-López, E. Synthesis and Characterization of Some New Tetraaldehyde and Tetraketone Derivatives and X-ray Structure of 1,1'-(4,4'-(2- (1,3-bis(4-Acetylphenoxy)propan-2-ylidene)propane-1,3-diyl) bis(oxy)bis(4,1-phenylene))diethanone. Int. J. Mol. Sci. 2008, 9, 1000-1007.

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