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Preparation and Characterization of Double Metal Cyanide Complex Catalysts
School of Chemistry and Environmental Science, University of Jinan, Jinan 250022, Shandong Province, P. R. China
School of Polymer Science and Tchnology, Qingdao University of Science and Technology, Qingdao, 266042, Shandong Province, P. R. China
* Author to whom correspondence should be addressed.
Received: 1 January 2003 / Accepted: / Published: 31 January 2003
Abstract: A series of double metal cyanide (DMC) complex catalysts were prepared in two different methods by using ß-cyclodextrin, PEG-1000 and Tween-60 as an additional complex ligands respectively. It was showed that a mixture of crystalline and amorphous DMC was synthesized by using traditional method in which the additional complex ligand was added after the precipitation of DMC. Amorphous and dispersed DMC with higher activity could be obtained when the additional complex ligand was added in the reactant solution before reaction. The effect of additional complex ligand and preparation method on the crystalline state and catalytic property of DMC were also investigated.
Keywords: Double metal cyanide complex; Catalysts; Preparation; Additional complex ligand
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MDPI and ACS Style
Liu, H.; Wang, X.; Gu, Y.; Guo, W. Preparation and Characterization of Double Metal Cyanide Complex Catalysts. Molecules 2003, 8, 67-73.
Liu H, Wang X, Gu Y, Guo W. Preparation and Characterization of Double Metal Cyanide Complex Catalysts. Molecules. 2003; 8(1):67-73.
Liu, Hanxia; Wang, Xikui; Gu, Yao; Guo, Weilin. 2003. "Preparation and Characterization of Double Metal Cyanide Complex Catalysts." Molecules 8, no. 1: 67-73.