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Molecules 2017, 22(5), 737; doi:10.3390/molecules22050737

Synthesis, Crystal Structures and Properties of Ferrocenyl Bis-Amide Derivatives Yielded via the Ugi Four-Component Reaction

College of Chemistry, Chemical Engineering and Materials Science, Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong, Shandong Normal University, Jinan 250014, China
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Academic Editor: Roman Dembinski
Received: 29 March 2017 / Revised: 21 April 2017 / Accepted: 27 April 2017 / Published: 4 May 2017
(This article belongs to the Section Organic Synthesis)
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Abstract

Ten ferrocenyl bis-amide derivatives were successfully synthesized via the Ugi four-component reaction by treating ferrocenecarboxylic acid with diverse aldehydes, amines, and isocyanides in methanol solution. Their chemical structures were fully characterized by IR, NMR, HR-MS, and X-ray diffraction analyses. They feature unique molecular morphologies and create a 14-membered ring motif in the centro-symmetric dimers generated in the solid state. Moreover, the electrochemical behavior of these ferrocenyl bis-amides was assessed by cyclic voltammetry. View Full-Text
Keywords: ferrocenyl bis-amide; Ugi four-component reaction; synthesis; crystal structure; cyclic voltammetry ferrocenyl bis-amide; Ugi four-component reaction; synthesis; crystal structure; cyclic voltammetry
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MDPI and ACS Style

Zhao, M.; Shao, G.-K.; Huang, D.-D.; Lv, X.-X.; Guo, D.-S. Synthesis, Crystal Structures and Properties of Ferrocenyl Bis-Amide Derivatives Yielded via the Ugi Four-Component Reaction. Molecules 2017, 22, 737.

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