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Molecules 2012, 17(4), 4209-4218; doi:10.3390/molecules17044209

Synthesis and NMR Spectral Studies of the 7-C60-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine

1
College of Chemical Engineering, Nanjing Forestry University, Nanjing 210037, China
2
College of Life and Environmental Sciences, Kaili University, Kaili, Guizhou 556011, China
*
Author to whom correspondence should be addressed.
Received: 4 March 2012 / Revised: 25 March 2012 / Accepted: 27 March 2012 / Published: 5 April 2012
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Abstract

The 7-C60-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The 1H-NMR and 13C-NMR resonance signals of the new compound are unambiguously assigned by using homo- and heteronuclear 2D NMR spectroscopic techniques such as COSY, ROESY, HSQC and HMBC. The C1 symmetric structure with 6,6-junction of compound was determined.
Keywords: 7-C60-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine; 1H-NMR; 13C-NMR; 2D NMR; C1 symmetric structure 7-C60-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine; 1H-NMR; 13C-NMR; 2D NMR; C1 symmetric structure
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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MDPI and ACS Style

Zhou, Z.; Lin, Z. Synthesis and NMR Spectral Studies of the 7-C60-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine. Molecules 2012, 17, 4209-4218.

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