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Molecules 2012, 17(4), 4209-4218; doi:10.3390/molecules17044209
Article

Synthesis and NMR Spectral Studies of the 7-C60-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine

1,2,*  and 1
1 College of Chemical Engineering, Nanjing Forestry University, Nanjing 210037, China 2 College of Life and Environmental Sciences, Kaili University, Kaili, Guizhou 556011, China
* Author to whom correspondence should be addressed.
Received: 4 March 2012 / Revised: 25 March 2012 / Accepted: 27 March 2012 / Published: 5 April 2012
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Abstract

The 7-C60-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The 1H-NMR and 13C-NMR resonance signals of the new compound are unambiguously assigned by using homo- and heteronuclear 2D NMR spectroscopic techniques such as COSY, ROESY, HSQC and HMBC. The C1 symmetric structure with 6,6-junction of compound was determined.
Keywords: 7-C60-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine; 1H-NMR; 13C-NMR; 2D NMR; C1 symmetric structure 7-C60-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine; 1H-NMR; 13C-NMR; 2D NMR; C1 symmetric structure
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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MDPI and ACS Style

Zhou, Z.; Lin, Z. Synthesis and NMR Spectral Studies of the 7-C60-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine. Molecules 2012, 17, 4209-4218.

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