Molecules 2010, 15(7), 4750-4756; doi:10.3390/molecules15074750
Article

Synthesis, Characterization and Reactivity Ratio Study of Poly(di(tri-n-butyltin) citraconate-co-N-vinylimidazole)

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Received: 13 June 2010; in revised form: 28 June 2010 / Accepted: 30 June 2010 / Published: 7 July 2010
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Abstract: The organotin monomer di(tri-n-butyltin) citraconate (DTBTC, I) was synthesized. Subsequently this monomer was copolymerized with N-vinylimidazole (VI) using a free radical technique. The overall conversion was kept low (≤14% wt/wt) for all studied samples and the copolymer composition was determined from tin analysis using the Gilman and Rosenberg method. The synthesized monomer and copolymer were further characterized by elemental analysis, 1H- and 13C-NMR, and FTIR spectroscopy.
Keywords: bis(tri-n-butyltin) oxide; citraconate; N-vinyl imidazole; reactivity ratio
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MDPI and ACS Style

Al-Deyab, S.S.; El-Newehy, M.H.; Al-Hazmi, A.M. Synthesis, Characterization and Reactivity Ratio Study of Poly(di(tri-n-butyltin) citraconate-co-N-vinylimidazole). Molecules 2010, 15, 4750-4756.

AMA Style

Al-Deyab SS, El-Newehy MH, Al-Hazmi AM. Synthesis, Characterization and Reactivity Ratio Study of Poly(di(tri-n-butyltin) citraconate-co-N-vinylimidazole). Molecules. 2010; 15(7):4750-4756.

Chicago/Turabian Style

Al-Deyab, Salem S.; El-Newehy, Mohamed H.; Al-Hazmi, Ali M. 2010. "Synthesis, Characterization and Reactivity Ratio Study of Poly(di(tri-n-butyltin) citraconate-co-N-vinylimidazole)." Molecules 15, no. 7: 4750-4756.


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