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Molecules 2010, 15(7), 4750-4756; doi:10.3390/molecules15074750
Article

Synthesis, Characterization and Reactivity Ratio Study of Poly(di(tri-n-butyltin) citraconate-co-N-vinylimidazole)

* , *  and
Petrochemical Research Chair, Chemistry Department, College of Science, King Saud University, Riyadh 11451, P.O. Box 2455, Saudi Arabia
* Authors to whom correspondence should be addressed.
Received: 13 June 2010 / Revised: 28 June 2010 / Accepted: 30 June 2010 / Published: 7 July 2010
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Abstract

The organotin monomer di(tri-n-butyltin) citraconate (DTBTC, I) was synthesized. Subsequently this monomer was copolymerized with N-vinylimidazole (VI) using a free radical technique. The overall conversion was kept low (≤14% wt/wt) for all studied samples and the copolymer composition was determined from tin analysis using the Gilman and Rosenberg method. The synthesized monomer and copolymer were further characterized by elemental analysis, 1H- and 13C-NMR, and FTIR spectroscopy.
Keywords: bis(tri-n-butyltin) oxide; citraconate; N-vinyl imidazole; reactivity ratio bis(tri-n-butyltin) oxide; citraconate; N-vinyl imidazole; reactivity ratio
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Al-Deyab, S.S.; El-Newehy, M.H.; Al-Hazmi, A.M. Synthesis, Characterization and Reactivity Ratio Study of Poly(di(tri-n-butyltin) citraconate-co-N-vinylimidazole). Molecules 2010, 15, 4750-4756.

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