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• El-Newehy, M
• Al-Hazmi, A
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• El-Newehy, M
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Molecules 2010, 15(7), 4750-4756; doi:10.3390/molecules15074750

Article

Synthesis, Characterization and Reactivity Ratio Study of Poly(di(tri-n-butyltin) citraconate-co-N-vinylimidazole)

Salem S. Al-Deyab* , Mohamed H. El-Newehy*  and Ali M. Al-Hazmi

Petrochemical Research Chair, Chemistry Department, College of Science, King Saud University, Riyadh 11451, P.O. Box 2455, Saudi Arabia

* Authors to whom correspondence should be addressed.

Received: 13 June 2010; in revised form: 28 June 2010 / Accepted: 30 June 2010 / Published: 7 July 2010

Download PDF Full-Text [127 KB, uploaded 7 July 2010 10:25 CEST]

Abstract: The organotin monomer di(tri-n-butyltin) citraconate (DTBTC, I) was synthesized. Subsequently this monomer was copolymerized with N-vinylimidazole (VI) using a free radical technique. The overall conversion was kept low (≤14% wt/wt) for all studied samples and the copolymer composition was determined from tin analysis using the Gilman and Rosenberg method. The synthesized monomer and copolymer were further characterized by elemental analysis, ¹H- and ¹³C-NMR, and FTIR spectroscopy.

Keywords: bis(tri-n-butyltin) oxide; citraconate; N-vinyl imidazole; reactivity ratio

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