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Synthesis of New Bis-1,2,4-Triazole Derivatives
Department of Chemistry, Giresun Faculty of Arts and Sciences, Karadeniz Technical University, 28049, Giresun, Turkey
* Author to whom correspondence should be addressed.
Received: 10 May 2006; in revised form: 20 June 2006 / Accepted: 21 June 2006 / Published: 21 June 2006
Abstract: A series of new 1,2/1,3-bis[o-(N-methylidenamino-3-aryl-5-phenyl-4H-1,2,4-triazole-4-yl)phenoxy]ethane/propane derivatives 4 were prepared in good yields bytreatment of 4-amino-3-aryl-5-phenyl-4H-1,2,4-triazoles 2 with certain bis-aldehydes 1.Compounds 4 were reduced with NaBH4 to afford the corresponding 1,2/1,3-bis[o-(N-methylamino-3-aryl-5-phenyl-4H-1,2,4-triazole-4-yl)phenoxy]ethane/propane derivatives5. All new compounds were characterized by IR, 1H-NMR, 13C-NMR and mass spectraldata.
Keywords: 4-Amino-4H-1; 2; 4-triazoles; bis-1; 2; 4-triazoles; bis-Schiff bases; bis- aldehydes
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Bekircan, O.; Bektas, H. Synthesis of New Bis-1,2,4-Triazole Derivatives. Molecules 2006, 11, 469-477.
Bekircan O, Bektas H. Synthesis of New Bis-1,2,4-Triazole Derivatives. Molecules. 2006; 11(6):469-477.
Bekircan, Olcay; Bektas, Hakan. 2006. "Synthesis of New Bis-1,2,4-Triazole Derivatives." Molecules 11, no. 6: 469-477.