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Polymers 2018, 10(5), 544; https://doi.org/10.3390/polym10050544

Hybrid Materials Based on Poly-3-amine-7-methylamine-2-methylphenazine and Magnetite Nanoparticles Immobilized on Single-Walled Carbon Nanotubes

1
A.V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, 29 Leninsky Prospect, Moscow 119991, Russia
2
Department of Chemistry, Lomonosov Moscow State University, 1-3 Leninskie Gory, Moscow 119991, Russia
3
Department of Functional Nanosystems and High-Temperature Materials, National University of Science and Technology MISIS, Leninsky Prospect, Moscow 119049, Russia
*
Author to whom correspondence should be addressed.
Received: 28 April 2018 / Revised: 14 May 2018 / Accepted: 15 May 2018 / Published: 18 May 2018
(This article belongs to the Special Issue Polymer Hybrid Materials)
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Abstract

Polymer-metal-carbon hybrid nanomaterials based on thermostable electroactive poly-3-amine-7-methylamine-2-methylphenazine (PAMMP), single walled carbon nanotubes (SWCNT), and magnetite (Fe3O4) nanoparticles were synthesized for the first time. Hybrid Fe3O4/SWCNT/PAMMP nanomaterial synthesis was carried out via in situ chemical oxidative polymerization of 3-amine-7-methylamine-2-methylphenazine hydrochloride in the presence of metal-carbon Fe3O4/SWCNT nanocomposites. Fe3O4/SWCNT nanocomposites were obtained by the immobilization of magnetite nanoparticles on the SWCNT surface in the course of Fe3O4 nanoparticles synthesis in alkaline medium. The developed nanocomposite materials were characterized by FTIR spectroscopy, X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission (FE-SEM) scanning electron microscopy, atomic absorption spectrometry (AAS), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and magnetometry. The chemical structure and phase composition, magnetic and electrical properties, and thermal stability of the obtained multifunctional nanomaterials, depending on synthesis conditions, were investigated. View Full-Text
Keywords: poly-3-amine-7-methylamine-2-methylphenazine; conjugated polymers; in situ oxidative polymerization; polymer-metal-carbon nanocomposite; single-walled carbon nanotubes; magnetite nanoparticles poly-3-amine-7-methylamine-2-methylphenazine; conjugated polymers; in situ oxidative polymerization; polymer-metal-carbon nanocomposite; single-walled carbon nanotubes; magnetite nanoparticles
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This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (CC BY 4.0).
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Zhiraslanovna Ozkan, S.; Petrovna Karpacheva, G.; Aleksandrovich Chernavskii, P.; Leont’evna Dzidziguri, E.; Nikolaevna Bondarenko, G.; Viktorovna Pankina, G. Hybrid Materials Based on Poly-3-amine-7-methylamine-2-methylphenazine and Magnetite Nanoparticles Immobilized on Single-Walled Carbon Nanotubes. Polymers 2018, 10, 544.

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