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Molecules 2002, 7(12), 867-870; doi:10.3390/71200867
Article

Microwave-Accelerated Iodination of Some Aromatic Amines, Using Urea-Hydrogen Peroxide Addition Compound (UHP) as the Oxidant

 and *
Received: 15 October 2002; in revised form: 11 December 2002 / Accepted: 12 December 2002 / Published: 31 December 2002
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Abstract: A fast and simple method for the oxidative iodination of some aromatic amines, under microwave irradiation, is reported, using diiodine and the the strongly Hbonded urea-hydrogen peroxide addition compound (H2NCONH2···H2O2, UHP) as the oxidant. The reactions were carried out in boiling CHCl3 under a reflux condenser to afford, within 10 minutes, the purified monoiodinated products in 40-80% yields.
Keywords: Monoiodinated arylamines; urea-hydrogen peroxide as oxidant; microwave irradiation Monoiodinated arylamines; urea-hydrogen peroxide as oxidant; microwave irradiation
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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MDPI and ACS Style

Sosnowski, M.; Skulski, L. Microwave-Accelerated Iodination of Some Aromatic Amines, Using Urea-Hydrogen Peroxide Addition Compound (UHP) as the Oxidant. Molecules 2002, 7, 867-870.

AMA Style

Sosnowski M, Skulski L. Microwave-Accelerated Iodination of Some Aromatic Amines, Using Urea-Hydrogen Peroxide Addition Compound (UHP) as the Oxidant. Molecules. 2002; 7(12):867-870.

Chicago/Turabian Style

Sosnowski, Maciej; Skulski, Lech. 2002. "Microwave-Accelerated Iodination of Some Aromatic Amines, Using Urea-Hydrogen Peroxide Addition Compound (UHP) as the Oxidant." Molecules 7, no. 12: 867-870.


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