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Molecules 2008, 13(5), 1120-1134; doi:10.3390/molecules13051120
Article

Synthesis of an ent-Halimanolide from ent-Halimic Acid

1,* , 1, 1, 1, 1, 2,3 and 1
1 Departamento de Química Orgánica, Universidad de Salamanca, Plaza de los Caídos 1-5, 37008 Salamanca, Spain 2 Centro de Investigación del Cáncer, Instituto de Biología Molecular y Celular del Cáncer, Consejo Superior de Investigaciones Científicas-Universidad de Salamanca, Campus Miguel de Unamuno, E-37007 Salamanca, Spain 3 APOINTECH, Campus Miguel de Unamuno, E-37007 Salamanca, Spain
* Author to whom correspondence should be addressed.
Received: 28 April 2008 / Revised: 7 May 2008 / Accepted: 7 May 2008 / Published: 9 May 2008
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Abstract

An efficient synthesis of ent-halimanolide 2 (15,16-epoxy-12-oxo-ent-halima- 5(10),13(16),14-trien-18,2β-olide), from ent-halimic acid has been achieved, corroborating the structure of the natural compound and establishing its absolute configuration.
Keywords: Ent-halimanolides; ent-halimic acid; diterpenoids; Cladogynos orientalis. Ent-halimanolides; ent-halimic acid; diterpenoids; Cladogynos orientalis.
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).
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Marcos, I.S.; Conde, A.; Moro, R.F.; Basabe, P.; Díez, D.; Mollinedo, F.; Urones, J.G. Synthesis of an ent-Halimanolide from ent-Halimic Acid. Molecules 2008, 13, 1120-1134.

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