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Molecules 2008, 13(10), 2601-2607; doi:10.3390/molecules13102601
Article

The Synthesis of 1-(4-Triethoxysilyl)phenyl)-4,4,4-trifluoro-1,3-butanedione, a Novel Trialkoxysilane Monomer for the Preparation of Functionalized Sol-gel Matrix Materials

,  and *
800 South Tucker Drive, Department of Chemistry and Biochemistry, The University of Tulsa, Tulsa, Oklahoma, 74104, USA
* Author to whom correspondence should be addressed.
Received: 23 September 2008 / Revised: 3 October 2008 / Accepted: 7 October 2008 / Published: 20 October 2008
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Abstract

The title compound, 1-(4-triethoxysilyl)phenyl)-4,4,4-trifluoro-1,3-butanedione, was synthesized in a three-step sequence starting from 2-(4-bromophenyl)propene. Containing both a trialkoxysilyl and a substituted 1,3-butanedione functional grouping within its structure, this new silane is a viable starting material for the preparation of functionalized sol-gel materials.
Keywords: Trialkoxysilane; 4; 4; 4-Trifluoro-1-phenyl-1; 3-butanedione (4-TPB); Sol-gel; Molecular imprinting Trialkoxysilane; 4; 4; 4-Trifluoro-1-phenyl-1; 3-butanedione (4-TPB); Sol-gel; Molecular imprinting
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Peeples, C.J.; Earni, R.R.; DiCesare, J.C. The Synthesis of 1-(4-Triethoxysilyl)phenyl)-4,4,4-trifluoro-1,3-butanedione, a Novel Trialkoxysilane Monomer for the Preparation of Functionalized Sol-gel Matrix Materials. Molecules 2008, 13, 2601-2607.

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