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An Efficient Scalable Synthesis of 2,3-Epoxypropyl Phenylhydrazones
Department of Organic Chemistry, Kaunas University of Technology, LT-50270 Kaunas, Lithuania
* Author to whom correspondence should be addressed.
Received: 3 January 2005; in revised form: 16 December 2005 / Accepted: 17 December 2005 / Published: 31 January 2006
Abstract: A series of mono and di-N-2,3-epoxypropyl N-phenylhydrazones have beenprepared on a large scale by reaction of the corresponding N-phenylhydrazones of9-ethyl-3-carbazolecarbaldehyde, 9-ethyl-3,6-carbazoledicarbaldehyde, 4-dimethyl-amino-, 4-diethylamino-, 4-benzylethylamino-, 4-(diphenylamino)-, 4-(4,4-4'-dimethyl-diphenylamino)-, 4-(4-formyldiphenylamino)- and 4-(4-formyl-4'-methyldiphenyl-amino)benzaldehyde with epichlorohydrin in the presence of KOH and anhydrousNa2SO4.
Keywords: Heterocycles; epichlorohydrin; hydrazones; charge transport.
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MDPI and ACS Style
Getautis, V.; Daskeviciene, M.; Malinauskas, T.; Stanisauskaite, A.; Stumbraite, J. An Efficient Scalable Synthesis of 2,3-Epoxypropyl Phenylhydrazones. Molecules 2006, 11, 64-71.
Getautis V, Daskeviciene M, Malinauskas T, Stanisauskaite A, Stumbraite J. An Efficient Scalable Synthesis of 2,3-Epoxypropyl Phenylhydrazones. Molecules. 2006; 11(1):64-71.
Getautis, Vytautas; Daskeviciene, Maryte; Malinauskas, Tadas; Stanisauskaite, Albina; Stumbraite, Jolanta. 2006. "An Efficient Scalable Synthesis of 2,3-Epoxypropyl Phenylhydrazones." Molecules 11, no. 1: 64-71.