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Molecules 2006, 11(1), 64-71; doi:10.3390/11010064
Article

An Efficient Scalable Synthesis of 2,3-Epoxypropyl Phenylhydrazones

* , , ,  and
Department of Organic Chemistry, Kaunas University of Technology, LT-50270 Kaunas, Lithuania
* Author to whom correspondence should be addressed.
Received: 3 January 2005 / Revised: 16 December 2005 / Accepted: 17 December 2005 / Published: 31 January 2006
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Abstract

A series of mono and di-N-2,3-epoxypropyl N-phenylhydrazones have beenprepared on a large scale by reaction of the corresponding N-phenylhydrazones of9-ethyl-3-carbazolecarbaldehyde, 9-ethyl-3,6-carbazoledicarbaldehyde, 4-dimethyl-amino-, 4-diethylamino-, 4-benzylethylamino-, 4-(diphenylamino)-, 4-(4,4-4'-dimethyl-diphenylamino)-, 4-(4-formyldiphenylamino)- and 4-(4-formyl-4'-methyldiphenyl-amino)benzaldehyde with epichlorohydrin in the presence of KOH and anhydrousNa2SO4.
Keywords: Heterocycles; epichlorohydrin; hydrazones; charge transport. Heterocycles; epichlorohydrin; hydrazones; charge transport.
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).
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Getautis, V.; Daskeviciene, M.; Malinauskas, T.; Stanisauskaite, A.; Stumbraite, J. An Efficient Scalable Synthesis of 2,3-Epoxypropyl Phenylhydrazones. Molecules 2006, 11, 64-71.

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