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Molecules 2006, 11(1), 64-71; doi:10.3390/11010064
Article

An Efficient Scalable Synthesis of 2,3-Epoxypropyl Phenylhydrazones

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Received: 3 January 2005 / Revised: 16 December 2005 / Accepted: 17 December 2005 / Published: 31 January 2006
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Abstract

A series of mono and di-N-2,3-epoxypropyl N-phenylhydrazones have beenprepared on a large scale by reaction of the corresponding N-phenylhydrazones of9-ethyl-3-carbazolecarbaldehyde, 9-ethyl-3,6-carbazoledicarbaldehyde, 4-dimethyl-amino-, 4-diethylamino-, 4-benzylethylamino-, 4-(diphenylamino)-, 4-(4,4-4'-dimethyl-diphenylamino)-, 4-(4-formyldiphenylamino)- and 4-(4-formyl-4'-methyldiphenyl-amino)benzaldehyde with epichlorohydrin in the presence of KOH and anhydrousNa2SO4.
Keywords: Heterocycles; epichlorohydrin; hydrazones; charge transport. Heterocycles; epichlorohydrin; hydrazones; charge transport.
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Getautis, V.; Daskeviciene, M.; Malinauskas, T.; Stanisauskaite, A.; Stumbraite, J. An Efficient Scalable Synthesis of 2,3-Epoxypropyl Phenylhydrazones. Molecules 2006, 11, 64-71.

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