Molecules 2005, 10(10), 1325-1334; doi:10.3390/10101325
Article

Facile Preparation of Peracetates and Per-3-bromobenzoates of α-Mono- and Disaccharides

Department of Chemistry, School of Sciences and Computer Engineering, University of Houston-Clear Lake, 2700 Bay Area Boulevard, Houston, TX 77058, USA
* Author to whom correspondence should be addressed.
Received: 1 July 2005; in revised form: 12 July 2005 / Accepted: 12 July 2005 / Published: 31 October 2005
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Abstract: A simple and convenient method for the preparation of fully acetylated and (3- bromo)benzoylated α-monosaccharides and disaccharides through vigorous mechanical mixing of solid reactants on a high speed shaker is described. Using this technique a variety of α-acylated sugars are prepared, including penta-O-acetyl-α-D-galactopyranose, penta-O- acetyl-α-D-glucopyranose, penta-O-acetyl-α-D-mannopyranose, octa-O-acetyl-α-lactose, penta-O-(3-bromo)benzoyl-α-D-galactopyranose, penta-O-(3-bromo)benzoyl-α-D-gluco- pyranose, penta-O-(3-bromo)benzoyl-α-D-mannopyranose, and octa-O-(3-bromo)benzoyl- α-lactose.
Keywords: α-Galactose; α-glucose; α-mannose; lactose; mechanochemical mixing

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MDPI and ACS Style

Wang, Z.(.; Matin, M.; Sheikh, S. Facile Preparation of Peracetates and Per-3-bromobenzoates of α-Mono- and Disaccharides. Molecules 2005, 10, 1325-1334.

AMA Style

Wang Z(, Matin M, Sheikh S. Facile Preparation of Peracetates and Per-3-bromobenzoates of α-Mono- and Disaccharides. Molecules. 2005; 10(10):1325-1334.

Chicago/Turabian Style

Wang, Zerong (Daniel); Matin, Mahfuza; Sheikh, Samia. 2005. "Facile Preparation of Peracetates and Per-3-bromobenzoates of α-Mono- and Disaccharides." Molecules 10, no. 10: 1325-1334.

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