Joint Forces of HR-Spicp-MS and EAF4-MALS for Characterization of Gold Nanorods Conjugated with Synthetic Glycopolymers †
Abstract
:1. Introduction
2. Materials and Methods
2.1. Glycopolymer Conjugated Gold Nanorods
2.2. HR-Spicp-MS
2.3. EAF4-MALS
3. Results
3.1. HR-spICP-MS for Glycoconjugated GNRs Characterization
3.2. EAF4-MALS for Glycoconjugated GNRs Characterization
4. Conclusions
Author Contributions
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
References
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Parameter | |
---|---|
RF power | 1300 W |
Plasma gas flow rate | 13 L min−1 |
Carrier gas flow rate | 0.93 L min−1 |
Measurement mode | TRA |
Nuclide monitored | 197Au |
Dwell time | 40 µs |
Acquisition time | 60 s |
Nebulizer | MicroMist |
Spray chamber | Cyclonic |
GNRs | GNR-Gal-PHEA35 | GNR-Gal-PHEA60 | |
---|---|---|---|
Spherical equivalent diameter (nm) | 21.0 ± 0.5 | 21.0 ± 0.4 | 22.0 ± 0.0 |
GNRs | GNR-Gal-PHEA35 | GNR-Gal-PHEA60 | |
---|---|---|---|
Dh (nm) | 17.0 | 21.3 | 22.1 |
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Velimirovic, M.; Pancaro, A.; Mildner, R.; Georgiou, P.G.; Tirez, K.; Nelissen, I.; Johann, C.; Gibson, M.I.; Vanhaecke, F. Joint Forces of HR-Spicp-MS and EAF4-MALS for Characterization of Gold Nanorods Conjugated with Synthetic Glycopolymers. Mater. Proc. 2021, 4, 93. https://doi.org/10.3390/IOCN2020-07923
Velimirovic M, Pancaro A, Mildner R, Georgiou PG, Tirez K, Nelissen I, Johann C, Gibson MI, Vanhaecke F. Joint Forces of HR-Spicp-MS and EAF4-MALS for Characterization of Gold Nanorods Conjugated with Synthetic Glycopolymers. Materials Proceedings. 2021; 4(1):93. https://doi.org/10.3390/IOCN2020-07923
Chicago/Turabian StyleVelimirovic, Milica, Alessia Pancaro, Robert Mildner, Panagiotis G. Georgiou, Kristof Tirez, Inge Nelissen, Christoph Johann, Matthew I. Gibson, and Frank Vanhaecke. 2021. "Joint Forces of HR-Spicp-MS and EAF4-MALS for Characterization of Gold Nanorods Conjugated with Synthetic Glycopolymers" Materials Proceedings 4, no. 1: 93. https://doi.org/10.3390/IOCN2020-07923