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Nanomaterials 2017, 7(9), 239;

Synthesis of Au-Pd Bimetallic Nanoflowers for Catalytic Reduction of 4-Nitrophenol

The State Key Laboratory of Refractories and Metallurgy, School of Chemistry & Chemical Engineering, Wuhan University of Science and Technology, Wuhan 430081, China
Author to whom correspondence should be addressed.
Received: 19 July 2017 / Revised: 6 August 2017 / Accepted: 22 August 2017 / Published: 26 August 2017
(This article belongs to the Special Issue Noble Metal Nanoparticles in Catalysis)
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Due to the great potential to improve catalytic performance, gold (Au) and palladium (Pd) bimetallic catalysts have prompted structure-controlled synthesis of Au-Pd nanoalloys bounded by high-index facets. In this work, we prepared Au-Pd bimetallic nanoflowers (NFs) with a uniform size, well-defined dendritic morphology, and homogeneous alloy structure in an aqueous solution by seed-mediated synthesis. The prepared bimetallic NFs were fully characterized using a combination of transmission electron microscopy, Ultraviolet-Visible (UV-vis) spectroscopy, inductively coupled plasma optical emission spectroscopy, and cyclic voltammetry measurements. The catalytic activities of the prepared Au-Pd nanoparticles for 4-nitrophenol reduction were also investigated, and the activities are in the order of Au@Pd NFs > Au-Pd NFs (Au1Pd1 core) > Au-Pd NFs (Au core), which could be related to the content and exposed different reactive surfaces of Pd in alloys. This result clearly demonstrates that the superior activities of Au-Pd alloy nanodendrites could be attributed to the synergy between Au and Pd in catalysts. View Full-Text
Keywords: bimetallic nanoparticles; Au-Pd alloy; reduction; 4-nitrophenol bimetallic nanoparticles; Au-Pd alloy; reduction; 4-nitrophenol

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This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (CC BY 4.0).

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Ma, T.; Liang, F.; Chen, R.; Liu, S.; Zhang, H. Synthesis of Au-Pd Bimetallic Nanoflowers for Catalytic Reduction of 4-Nitrophenol. Nanomaterials 2017, 7, 239.

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