Preparation and Properties of Waterborne Epoxy-Resin-Emulsified Asphalt Modified by Oxidized Extraction Oil
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Preparation Process
2.2.1. Extraction Oil Oxidation Pretreatment
2.2.2. Preparation of Extraction Oil/Waterborne Epoxy Resin System
2.2.3. Preparation of Extraction Oil/Waterborne Epoxy-Resin-Emulsified Asphalt
2.3. Characterizations
3. Results and Discussion
3.1. Performance Analysis of Oxidized Extraction Oil
3.1.1. FTIR
3.1.2. Emulsion Properties Comparison of Extraction Oil before and after Oxidation
3.2. Extraction Oil/Waterborne Epoxy Resin System
3.2.1. Emulsion Properties
3.2.2. Viscosity
3.2.3. Mechanical Properties
3.2.4. Compatibility
3.3. Oxidized Extraction Oil/Waterborne Epoxy-Resin-Emulsified Asphalt System
3.3.1. Viscosity
3.3.2. Mechanical Properties
3.3.3. Aging Performance
3.3.4. Compatibility
3.3.5. Microstructure of Extracted Oil/WEREA during Curing
4. Conclusions
5. Limitations
Author Contributions
Funding
Conflicts of Interest
References
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Samples | Epoxy Resin | Curing Agent | Emulsified Asphalt | Oxidized Extraction Oil | Deionized Water |
---|---|---|---|---|---|
WEREA | 5 | 5 | 5 | 0 | 6.67 |
WEAO-4 | 5 | 5 | 5 | 4 | 9.33 |
WEAO-5 | 5 | 5 | 5 | 5 | 10 |
WEAO-6 | 5 | 5 | 5 | 6 | 10.67 |
WEAO-7 | 5 | 5 | 5 | 7 | 11.33 |
Properties | EO/WER Emulsion | OEO/WER Emulsion |
---|---|---|
Shear difficulty | Difficult | Easy |
Emulsion uniformity | Homogeneous | Non-homogeneous |
Stability | Layered, separated | Stable |
Samples | Shear Difficulty | Appearance | Drying Time/h | Film Forming Property | |
---|---|---|---|---|---|
Surface Dry Time | Real Drying Time | ||||
WER | Easy | Homogeneous, no-stratification | 4 | 22 | Good |
WEO-2 | Easy | Homogeneous, no-stratification | 4.2 | 22.3 | Good |
WEO-3 | Easy | Homogeneous, no-stratification | 4.8 | 23 | Good |
WEO-4 | Easy | Homogeneous, no-stratification | 5.3 | 23.5 | Good |
WEO-5 | Relatively easy | Relatively non-homogeneous slight segregation | 6 | 24.2 | Fairly good |
Samples | Tensile Strength (MPa) | Elongation at Break (%) | ||||
---|---|---|---|---|---|---|
Before Aging | After Aging | Loss Ratio | Before Aging | After Aging | Loss Ratio | |
WEREA | 5.36 | 4.91 | 8.4% | 62.12 | 53.61 | 13.7% |
WEAO-4 | 4.34 | 4.04 | 7.76% | 93.72 | 86.94 | 7.23% |
WEAO-5 | 3.85 | 3.57 | 7.27% | 102.25 | 96.24 | 5.9% |
WEAO-6 | 3.55 | 3.31 | 6.76% | 110.6 | 105.1 | 4.97% |
WEAO-7 | 3.32 | 3.12 | 6.02% | 105.88 | 100.86 | 4.74% |
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Ai, T.; Pang, H.; Wu, X.; Zhong, D.; Yang, K.; Yan, X.; Niu, Y. Preparation and Properties of Waterborne Epoxy-Resin-Emulsified Asphalt Modified by Oxidized Extraction Oil. Buildings 2022, 12, 2133. https://doi.org/10.3390/buildings12122133
Ai T, Pang H, Wu X, Zhong D, Yang K, Yan X, Niu Y. Preparation and Properties of Waterborne Epoxy-Resin-Emulsified Asphalt Modified by Oxidized Extraction Oil. Buildings. 2022; 12(12):2133. https://doi.org/10.3390/buildings12122133
Chicago/Turabian StyleAi, Tao, Hua Pang, Xuanxuan Wu, Danni Zhong, Kun Yang, Xin Yan, and Yanhui Niu. 2022. "Preparation and Properties of Waterborne Epoxy-Resin-Emulsified Asphalt Modified by Oxidized Extraction Oil" Buildings 12, no. 12: 2133. https://doi.org/10.3390/buildings12122133