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Crystals 2017, 7(10), 290; doi:10.3390/cryst7100290

Synthesis and X-ray Crystal Structure of N’-Cyano-N,N’-dimethyl-4-nitrobenzohydrazide

1
Helmholtz-Zentrum Dresden-Rossendorf, Institut für Radiopharmazeutische Krebsforschung, Bautzner Landstraße 400, D-01328 Dresden, Germany
2
Anorganische Festkörperchemie, Institut für Chemie, Universität Rostock, Albert-Einstein-Straße 3a, D-18059 Rostock, Germany
*
Author to whom correspondence should be addressed.
Academic Editor: Shujun Zhang
Received: 29 August 2017 / Revised: 18 September 2017 / Accepted: 19 September 2017 / Published: 26 September 2017
(This article belongs to the Section Crystal Engineering)
View Full-Text   |   Download PDF [2107 KB, uploaded 26 September 2017]   |  

Abstract

Using a two-step procedure, N’-cyano-N,N’-dimethyl-4-nitrobenzohydrazide was synthesized. The structure was established using single crystal X-ray diffraction. It crystalized in the orthorhombic space group P212121 where a = 8.1974(6), b = 10.6696(7), and c = 12.9766(8) Å. The first reported crystal structure of an acyclic cyanohydrazide is discussed with a focus on the geometry of the hydrazide moiety, but intermolecular contacts in the crystal are also considered. View Full-Text
Keywords: N,N’-diacylhydrazines; cyanamides; X-ray structure; resonance electron transfer; enzyme inhibition; bioconjugation N,N’-diacylhydrazines; cyanamides; X-ray structure; resonance electron transfer; enzyme inhibition; bioconjugation
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This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (CC BY 4.0).

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Löser, R.; Pitzschler, R.; Köckerling, M. Synthesis and X-ray Crystal Structure of N’-Cyano-N,N’-dimethyl-4-nitrobenzohydrazide. Crystals 2017, 7, 290.

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