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Crystals 2015, 5(4), 466-474; doi:10.3390/cryst5040466

Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid

Leibniz Institute for Catalysis at the University of Rostock (LIKAT), Albert-Einstein-Str. 29a, D-18059 Rostock, Germany
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Academic Editor: Helmut Cölfen
Received: 25 September 2015 / Revised: 9 October 2015 / Accepted: 10 October 2015 / Published: 16 October 2015
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Abstract

The molecular structures of (E)-non-2-enoic acid (C9) and (E)-dec-2-enoic acid (C10) are reported. The title compounds were crystallized by slow evaporation of ethanolic solutions at −30 °C. C9 crystallizes in the monoclinic space group P21/c and C10 in the triclinic space group P-1, each with 4 molecules in the unit cell. The unit cell parameters for C9 are: a = 10.6473(4) Å, b = 5.2855(2) Å, c = 17.0313(7) Å; β = 106.0985(10)° and V = 920.87(6) Å3. The unit cell parameters for C10 are: a = 4.1405(2) Å, b = 15.2839(6) Å, c = 17.7089(7) Å; α = 68.3291(11)°, β = 83.3850(13)°, γ = 85.0779(12)° and V = 1033.39(8) Å3. View Full-Text
Keywords: X-ray crystal structure; hydrogen bond; dimer; unsaturated carboxylic acid; fatty acid X-ray crystal structure; hydrogen bond; dimer; unsaturated carboxylic acid; fatty acid
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (CC BY 4.0).

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MDPI and ACS Style

Sonneck, M.; Peppel, T.; Spannenberg, A.; Wohlrab, S. Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid. Crystals 2015, 5, 466-474.

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