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Crystals 2011, 1(2), 34-39; doi:10.3390/cryst1020034

Synthesis and Crystal Structure of 1-(3-fluorophenyl)-3-(3,4,5-trimethoxybenzoyl)thiourea

1
Department of Chemistry, Quaid-I-Azam University, Islamabad 45320, Pakistan
2
Institut für Anorganische Chemie, J.-W.-Goethe-Universität, Max-von-Laue-Str.7, D-60438 Frankfurt/Main, Germany
*
Author to whom correspondence should be addressed.
Received: 28 March 2011 / Revised: 25 April 2011 / Accepted: 4 May 2011 / Published: 9 May 2011
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Abstract

The title thiourea was synthesized by reaction of 3,4,5-trimethoxybenzoyl isothiocyante with 3-fluoroaniline. The 3,4,5-trimethoxybenzoyl isothiocyante was produced in situ by reaction of 3,4,5-trimethoxybenzoyl chloride with ammonium thiocyanate in dry acetonitrile. The structure was confirmed by the spectroscopic, elemental analysis and single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P21/c with unit cell dimensions a = 13.0966(9), b = 16.6460(13), c = 7.8448(5), β = 106.721(5)°, V 1637.9(2) ų, Z = 4.
Keywords: Synthesis; 1-(3-fluorophenyl)-3-(3,4,5-trimethoxybenzoyl)thiourea; crystal structure Synthesis; 1-(3-fluorophenyl)-3-(3,4,5-trimethoxybenzoyl)thiourea; crystal structure
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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MDPI and ACS Style

Saeed, A.; Shaheen, U.; Bolte, M. Synthesis and Crystal Structure of 1-(3-fluorophenyl)-3-(3,4,5-trimethoxybenzoyl)thiourea. Crystals 2011, 1, 34-39.

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