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Molbank 2018, 2018(1), M977; https://doi.org/10.3390/M977

5-Amino-3-methyl-1,2,4-thiadiazole

EaStCHEM School of Chemistry, University of St Andrews, North Haugh, St Andrews, Fife KY16 9ST, UK
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Received: 12 December 2017 / Revised: 11 January 2018 / Accepted: 19 January 2018 / Published: 21 January 2018
(This article belongs to the Special Issue Heterocycles)
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Abstract

An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C-NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules. View Full-Text
Keywords: 1,2,4-thiadiazole; NMR spectra; IR spectrum; X-ray structure 1,2,4-thiadiazole; NMR spectra; IR spectrum; X-ray structure
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This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (CC BY 4.0).

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Aitken, R.A.; Slawin, A.M.Z. 5-Amino-3-methyl-1,2,4-thiadiazole. Molbank 2018, 2018, M977.

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