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Molbank, Volume 2015, Issue 3 (September 2015)

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Open AccessShort Note Hexakis{4-[(4′-hydroxybiphenyl-4-yl)ethynyl]phenyl}benzene
Molbank 2015, 2015(3), M865; doi:10.3390/M865
Received: 13 May 2015 / Revised: 24 June 2015 / Accepted: 24 June 2015 / Published: 2 July 2015
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Abstract
A novel polyphenolic backbone, hexakis{4-[(4′-hydroxybiphenyl-4-yl)ethynyl]phenyl}benzene, was synthesised using a common synthetic protocol used for the synthesis of similar polyphenolic compounds. Full article
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Open AccessShort Note 3,4-Dihydro-3-(2-hydroxyethyl)-4-(nitromethyl)quinazolin-2(1H)-one
Molbank 2015, 2015(3), M866; doi:10.3390/M866
Received: 30 April 2015 / Revised: 30 June 2015 / Accepted: 1 July 2015 / Published: 10 July 2015
Cited by 2 | PDF Full-text (322 KB) | HTML Full-text | XML Full-text | Supplementary Files
Abstract
A one-pot, direct synthesis of 3,4-dihydro-3-(2-hydroxyethyl)-4-(nitromethyl)quinazolin-2(1H)-one from methyl (2-formylphenyl)carbamate, ethanolamine and nitromethane in AcOH is reported. The reaction proceeds via a cascade three-component aza-Henry reaction under microwave irradiation and the title compound was characterized by 1H NMR, 13C NMR and ESI/MS analysis. Full article
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Open AccessShort Note 1-(3-Amino-1-phenylpropyl)-3-(2-fluorophenyl)-1,3-dihydro-2H-benzimidazol-2-one
Molbank 2015, 2015(3), M867; doi:10.3390/M867
Received: 18 June 2015 / Revised: 17 August 2015 / Accepted: 18 August 2015 / Published: 21 August 2015
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Abstract
Starting from 1-(2-fluorophenyl)-1,3-dihydro-2H-benzimidazol-2-one (1) and (1-bromo-3-chloropropyl)benzene (2), the target compound 3, which represents a precursor for future radiolabeling, is prepared in a three-step synthesis. Full article
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