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Molbank, Volume 2014, Issue 4 (December 2014)

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Open AccessShort Note 4,5-Dimethylbenzene-1,2-dimethanol
Molbank 2014, 2014(4), M835; doi:10.3390/M835
Received: 25 September 2014 / Accepted: 10 October 2014 / Published: 17 October 2014
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An efficient and cost-effective synthesis of 4,5-dimethylbenzene-1,2-dimethanol is reported. The synthesis is accomplished in three steps with an overall yield of 80%. Full article

Open AccessShort Note N'-[2-(7,8-Dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethylidene]-4-nitrobenzohydrazide
Molbank 2014, 2014(4), M836; doi:10.3390/M836
Received: 6 August 2014 / Accepted: 23 October 2014 / Published: 28 October 2014
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The title compound, N'-[2-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin- 10(2H)-yl)ethylidene]-4-nitrobenzohydrazide (1), was obtained by the reaction of formylmethylflavin and p-nitrobenzohydrazide. The product 1 inhibited the DNA binding of nuclear factor-κB, and was characterized by 1H-NMR, 13C-NMR, electrospray ionization mass spectrometry, elemental analysis, IR and UV. Full article

Open AccessShort Note (2S)-[3-(Anthracen-9-yl)-4,5-dihydroisoxazol-5-yl]methyl 2-[(tert-butoxycarbonyl)amino]propanoate
Molbank 2014, 2014(4), M837; doi:10.3390/M837
Received: 4 September 2014 / Accepted: 25 November 2014 / Published: 28 November 2014
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The synthesis of the (2S)-[3-(anthracen-9-yl)-4,5-dihydroisoxazol-5-yl]methyl 2-[(tert-butoxycarbonyl)amino]propanoate is obtained through the 1,3-dipolar cycloaddition of the stable anthracenenitrile oxide and the N-Boc protected (S)-alanine allyl ester as dipolarophile. The structure and the fluorescence properties are described upon the relative analytical and spectroscopic data. Full article

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