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2-[2-(Aziridin-1-yl)ethyl]-5,5-dimethyl-2,5-dihydro-4H-benzo [e]isoindol-4-one (Cytotoxic Oxonaphthalene-Pyrroles, Part IV)
Molbank 2012, 2012(4), M782; doi:10.3390/M782
Short Note

3-Chloro-5-(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

 and *
Received: 24 September 2012 / Accepted: 12 October 2012 / Published: 16 October 2012
Download PDF [117 KB, 7 November 2012; original version 16 October 2012]

Abstract

3-Chloro-5-trifluoromethanesulfonate-4H-1,2,6-thiadiazin-4-one 3 reacts with (4-dodecylthiophen-2-yl)trimethylstannane 5 (1 equiv.) in the presence of Pd(Ph3P)2Cl2 (5 mol%) in benzene at ca. 20 °C for 5 h to give 3-chloro-5-(4-dodecylthien-2-yl)-1,2,6-thiadiazinone 6 in 87% yield.
Keywords: 1,2,6-thiadiazines; thiophenes; heterocycles; oligomers 1,2,6-thiadiazines; thiophenes; heterocycles; oligomers
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Ioannidou, H.A.; Koutentis, P.A. 3-Chloro-5-(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one. Molbank 2012, 2012, M782.

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