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Molbank 2010, 2010(2), M676; doi:10.3390/M676
Short Note

(E)-2-((4R,5R)-5-((Benzyloxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)but-2-ene-1,4-diol

1, 2, 2, 1, 3,4,*  and 1,*
Received: 11 March 2010 / Accepted: 14 April 2010 / Published: 19 April 2010
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Abstract

The synthesis of (E)-2-((4R,5R)-5-((benzyloxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)but-2-ene-1,4-diol by a one-step reduction of the appropriate 2-substituted butenolide is reported. Product characterization was carried out by IR, 1H NMR, 13C NMR, MS, elemental analysis and optical rotation.
Keywords: reduction; DIBAL-H; substituted butenolides; allylic diols reduction; DIBAL-H; substituted butenolides; allylic diols
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Carreras, C.R.; García, C.E.; Martín, V.S.; Tonn, C.E.; Díaz, D.D.; Ceñal, J.P. (E)-2-((4R,5R)-5-((Benzyloxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)but-2-ene-1,4-diol. Molbank 2010, 2010, M676.

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