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Molbank, Volume 1997, Issue 3 (June 1997)

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Open AccessShort Note [3S*,5S*,6S*]-1,7-Dioxaspiro[5.5]undecane-3,5-diyl Diacetate
Molecules 1997, 2(6), M22; https://doi.org/10.3390/M22
Received: 18 June 1997 / Published: 20 June 1997
| Supplementary Files
Abstract
To a solution of [3S*,5S*,6S*]-1,7-dioxaspiro[5.5]undecane-3,5-diol (1) [1] (33 mg, 0.17 mmol) in dichloromethane (10 ml) was added triethylamine (54 mg, 0.53 mmol), acetic anhydride (34 mg, 0.34 mmol) and 4-dimethylaminopyridine (3 mg).[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note [4R*,5R*,6S*]-1,7-Dioxaspiro[5.5]undec-4,5-diyl Diacetate
Molecules 1997, 2(6), M21; https://doi.org/10.3390/M21
Received: 18 June 1997 / Published: 20 June 1997
| Supplementary Files
Abstract
To a solution of [4R*,5R*,6S*]-1,7-dioxaspiro[5.5]undecane-4,5-diol (1) (50 mg, 0.27 mmol) in dichloromethane (10 ml) was added triethylamine (100 mg, 0.99 mmol), acetic anhydride (67 mg, 0.66 mmol) and 4-dimethylaminopyridine (3 mg).[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note [3S*,5S*,6S*]-1,7-Dioxaspiro[5.5]undecane-3,5-diol
Molecules 1997, 2(6), M20; https://doi.org/10.3390/M20
Received: 18 June 1997 / Published: 20 June 1997
Cited by 1 | Supplementary Files
Abstract
The reaction and the product ratio shown in the scheme was reported [1].[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note [4R*,5R*,6S*]-1,7-Dioxaspiro[5.5]undecane-4,5-diol
Molecules 1997, 2(6), M19; https://doi.org/10.3390/M19
Received: 18 June 1997 / Published: 20 June 1997
Cited by 1 | Supplementary Files
Abstract
A solution of [3R*,4R*,5S*,6S*]-3,4-epoxy-1,7-dioxaspiro[5.5]undecan-5-ol (1) (561 mg, 3.01mmol) in dry tetrahydrofuran (30 ml) under a nitrogen atmosphere was cooled to 0 deg.C in an ice/water bath.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note [3R*,5S*,6S*]-1,7-Dioxaspiro[5.5]undecane-3,5-diyl Bis(3,5-dinitrobenzoate)
Molecules 1997, 2(6), M18; https://doi.org/10.3390/M18
Received: 16 June 1997 / Published: 20 June 1997
| Supplementary Files
Abstract
To a solution of [3R*,5S8,6S*]-1,7-dioxaspiro[5.5]undecane-3,5-diol (50 mg, 0.27 mmol) in dichloromethane (5.0 cm3), was added triethylamine (60 mg, 0.59 mmol), 4-dimethylaminopyridine (~1 mg), 3,5-dinitrobenzoyl chloride (136 mg, 0.59 mmol) and the resultant solution allowed to stand at room temperature for 120 h.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note [3R*,5S*,6S*]-5-Hydroxy-1,7-dioxaspiro[5.5]undec-3-yl 3,5-Dinitrobenzoate
Molecules 1997, 2(6), M17; https://doi.org/10.3390/M17
Received: 16 June 1997 / Published: 20 June 1997
| Supplementary Files
Abstract
To a solution of [3R*,5S8,6S*]-1,7-dioxaspiro[5.5]undecane-3,5-diol (50 mg, 0.27 mmol) in dichloromethane (5.0 ml), was added triethylamine (56 mg, 0.55 mmol), 4-dimethylaminopyridine (~1 mg), and 3,5-dinitrobenzoyl chloride (64 mg, 0.28 mmol) and the resultant solution allowed to stand
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To a solution of [3R*,5S8,6S*]-1,7-dioxaspiro[5.5]undecane-3,5-diol (50 mg, 0.27 mmol) in dichloromethane (5.0 ml), was added triethylamine (56 mg, 0.55 mmol), 4-dimethylaminopyridine (~1 mg), and 3,5-dinitrobenzoyl chloride (64 mg, 0.28 mmol) and the resultant solution allowed to stand at room temperature for 48 h.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note [2R*,5S*,6S*]-2-Methyl-1,7-dioxaspiro[5.5]undec-2-en-5-ol
Molecules 1997, 2(6), M16; https://doi.org/10.3390/M16
Received: 16 June 1997 / Published: 20 June 1997
Cited by 1 | Supplementary Files
Abstract
The reaction and the product ratio shown in the scheme was reported [1] [...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note [2R*,5S*,6S*]-2-Methyl-1,7-dioxaspiro[5.5]undec-3-en-5-ol§
Molecules 1997, 2(6), M15; https://doi.org/10.3390/M15
Received: 16 June 1997 / Published: 20 June 1997
| Supplementary Files
Abstract
Isomerisations of epoxides to allylic alcohols have been effected by strong non-nucleophilic bases such as lithium dialkylamides.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note 2-Ethyl-1-hydroxymethyl-4-trifluoromethyl-9H-carbazole
Molecules 1997, 2(6), M14; https://doi.org/10.3390/M14
Received: 11 June 1997 / Published: 16 June 1997
| Supplementary Files
Abstract
The general part of the experimental section [1] has been presented elsewhere.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
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