Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene)

doi:10.3390/80200243

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Molecules 2003, 8(2), 243-250; doi:10.3390/80200243

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Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene)

Robert I. Haines * and Dean R. Hutchings

Department of Chemistry, University of Prince Edward Island, 550 University Avenue, Charlottetown, PE, C1A 4P3, Canada

* Author to whom correspondence should be addressed.

Received: 19 December 2002; in revised form: 12 January 2003 / Accepted: 13 January 2003 / Published: 28 February 2003

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Abstract: The pendant-arm macrocycle, meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene) has been synthesized and its single crystal structure determined. The molecule crystallizes in a primitive monoclinic cell, with the space group P2₁/_a (#14). The cell dimensions are a = 10.778(3)Å, b = 13.809(3) Å, c = 11.420(2) Å, = 102.49(2)°, volume = 1659.5(6) Å³.

Keywords: Pendant-arm macrocycle; crystal structure; 1-methylnaphthalene

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MDPI and ACS Style

Haines, R.I.; Hutchings, D.R. Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene). Molecules 2003, 8, 243-250.

AMA Style

Haines R.I., Hutchings D.R. Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene). Molecules. 2003; 8(2):243-250.

Chicago/Turabian Style

Haines, Robert I.; Hutchings, Dean R. 2003. "Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene)." Molecules 8, no. 2: 243-250.

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