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Molecules 2003, 8(2), 243-250; doi:10.3390/80200243

Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene)

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Received: 19 December 2002 / Revised: 12 January 2003 / Accepted: 13 January 2003 / Published: 28 February 2003
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The pendant-arm macrocycle, meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene) has been synthesized and its single crystal structure determined. The molecule crystallizes in a primitive monoclinic cell, with the space group P21/a (#14). The cell dimensions are a = 10.778(3)Å, b = 13.809(3) Å, c = 11.420(2) Å, = 102.49(2)°, volume = 1659.5(6) Å3.
Keywords: Pendant-arm macrocycle; crystal structure; 1-methylnaphthalene Pendant-arm macrocycle; crystal structure; 1-methylnaphthalene
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Haines, R.I.; Hutchings, D.R. Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene). Molecules 2003, 8, 243-250.

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