Next Article in Journal
Regioselective Ethanolamination and Ketalization of 3-Ph-2,4-diacetyl(diethoxycarbonyl)-5-hydroxy-5-methylcyclohexanones
Previous Article in Journal
The 3-Attractor Water Model: Monte-Carlo Simulations with a New, Effective 2-Body Potential (BMW)
Molecules 2003, 8(2), 243-250; doi:10.3390/80200243
Article

Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene)

*  and
Department of Chemistry, University of Prince Edward Island, 550 University Avenue, Charlottetown, PE, C1A 4P3, Canada
* Author to whom correspondence should be addressed.
Received: 19 December 2002 / Revised: 12 January 2003 / Accepted: 13 January 2003 / Published: 28 February 2003
View Full-Text   |   Download PDF [76 KB, uploaded 18 June 2014]   |  

Abstract

The pendant-arm macrocycle, meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene) has been synthesized and its single crystal structure determined. The molecule crystallizes in a primitive monoclinic cell, with the space group P21/a (#14). The cell dimensions are a = 10.778(3)Å, b = 13.809(3) Å, c = 11.420(2) Å, = 102.49(2)°, volume = 1659.5(6) Å3.
Keywords: Pendant-arm macrocycle; crystal structure; 1-methylnaphthalene Pendant-arm macrocycle; crystal structure; 1-methylnaphthalene
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).
SciFeed

Share & Cite This Article

Further Mendeley | CiteULike
Export to BibTeX |
EndNote |
RIS
MDPI and ACS Style

Haines, R.I.; Hutchings, D.R. Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene). Molecules 2003, 8, 243-250.

View more citation formats

Related Articles

Article Metrics

For more information on the journal, click here

Comments

[Return to top]
Molecules EISSN 1420-3049 Published by MDPI AG, Basel, Switzerland RSS E-Mail Table of Contents Alert