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Molecules 2003, 8(2), 243-250; doi:10.3390/80200243
Article

Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene)

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Received: 19 December 2002 / Revised: 12 January 2003 / Accepted: 13 January 2003 / Published: 28 February 2003
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Abstract

The pendant-arm macrocycle, meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene) has been synthesized and its single crystal structure determined. The molecule crystallizes in a primitive monoclinic cell, with the space group P21/a (#14). The cell dimensions are a = 10.778(3)Å, b = 13.809(3) Å, c = 11.420(2) Å, = 102.49(2)°, volume = 1659.5(6) Å3.
Keywords: Pendant-arm macrocycle; crystal structure; 1-methylnaphthalene Pendant-arm macrocycle; crystal structure; 1-methylnaphthalene
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Haines, R.I.; Hutchings, D.R. Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene). Molecules 2003, 8, 243-250.

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