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Molecules 2014, 19(2), 2602-2611; doi:10.3390/molecules19022602
Article

Glycosylation of a Newly Functionalized Orthoester Derivative

, ,  and *
Received: 26 January 2014 / Revised: 20 February 2014 / Accepted: 21 February 2014 / Published: 24 February 2014
(This article belongs to the Section Organic Synthesis)
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Abstract

Tandem glycosylation of the 6-O-Fmoc-substituted benzyl orthoester derivative 2a was carried out in moderate yields by electrogenerated acid (EGA). The Fmoc group was effectively removed under mild basic conditions, and the product was submitted to the subsequent glycosylation.
Keywords: glycosylation; orthoester; electrogenerated acid (EGA); Fmoc group; selective deprotection glycosylation; orthoester; electrogenerated acid (EGA); Fmoc group; selective deprotection
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Kawa, K.; Saitoh, T.; Kaji, E.; Nishiyama, S. Glycosylation of a Newly Functionalized Orthoester Derivative. Molecules 2014, 19, 2602-2611.

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