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Molecules 2014, 19(2), 2602-2611; doi:10.3390/molecules19022602

Glycosylation of a Newly Functionalized Orthoester Derivative

Department of Chemistry, Faculty of Science and Technology, Keio University, Hiyoshi 3-14-1, Kohoku-ku, Yokohama 223-8522, Japan
Author to whom correspondence should be addressed.
Received: 26 January 2014 / Revised: 20 February 2014 / Accepted: 21 February 2014 / Published: 24 February 2014
(This article belongs to the Section Organic Synthesis)
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Tandem glycosylation of the 6-O-Fmoc-substituted benzyl orthoester derivative 2a was carried out in moderate yields by electrogenerated acid (EGA). The Fmoc group was effectively removed under mild basic conditions, and the product was submitted to the subsequent glycosylation.
Keywords: glycosylation; orthoester; electrogenerated acid (EGA); Fmoc group; selective deprotection glycosylation; orthoester; electrogenerated acid (EGA); Fmoc group; selective deprotection

This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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MDPI and ACS Style

Kawa, K.; Saitoh, T.; Kaji, E.; Nishiyama, S. Glycosylation of a Newly Functionalized Orthoester Derivative. Molecules 2014, 19, 2602-2611.

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