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Authors = Cemal Esen

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14 pages, 68479 KiB  
Article
Design Guide for Hybrid-Additive Manufacturing of Inconel 718 Combining PBF-LB/M and In Situ High-Speed Milling
by David Sommer, Simon Hornung, Cemal Esen and Ralf Hellmann
J. Manuf. Mater. Process. 2025, 9(3), 88; https://doi.org/10.3390/jmmp9030088 - 10 Mar 2025
Viewed by 1008
Abstract
As the correlation between design rules and process limitations is of the upmost importance for the full exploitation of any manufacturing technology, we report a design guide for hybrid-additive manufacturing of Inconel 718. Basic limitations need to be evaluated for this particular hybrid [...] Read more.
As the correlation between design rules and process limitations is of the upmost importance for the full exploitation of any manufacturing technology, we report a design guide for hybrid-additive manufacturing of Inconel 718. Basic limitations need to be evaluated for this particular hybrid approach that combines laser powder bed fusion (PBF-LB/M) and in situ high-speed milling. Fundamental geometric limitations are examined with regard to the minimum feasible wall thickness, cylinders, overhanging structures, and chamfers. Furthermore, geometrical restrictions due to the integrated three-axis milling process with respect to inclinations, inner angles, notches, and boreholes are investigated. From these findings, we derive design guidelines for a reliable build process using this hybrid manufacturing. Additionally, a design guideline for the hybrid-additive manufacturing approach is presented, depicting a step-to-step guide for the adjustment of constructions. To demonstrate this, a powder nozzle for a direct energy deposition (DED-LB/M) process is redesigned following the previously defined guidelines. This redesign encompasses analysis of the existing component and identification of problematic areas such as flat angles, leading to a new construction that is suitable for a hybrid-additive manufacturing approach. Full article
(This article belongs to the Special Issue Advances in Powder Bed Fusion Technologies)
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11 pages, 13063 KiB  
Article
Rheological Investigation of Highly Filled Copper(II) Oxide Nanosuspensions to Optimize Precursor Particle Content in Reductive Laser-Sintering
by Kay Bischoff, Dominik Mücke, Andreas Schubert, Cemal Esen and Ralf Hellmann
Liquids 2024, 4(2), 382-392; https://doi.org/10.3390/liquids4020019 - 24 Apr 2024
Cited by 1 | Viewed by 1164
Abstract
In this article, the particle concentration of finely dispersed copper(II) oxide nanosuspensions as precursors for reductive laser sintering (RLS) is optimized on the basis of rheological investigations. For this metallization process, a smooth, homogeneous and defect-free precursor layer is a prerequisite for adherent [...] Read more.
In this article, the particle concentration of finely dispersed copper(II) oxide nanosuspensions as precursors for reductive laser sintering (RLS) is optimized on the basis of rheological investigations. For this metallization process, a smooth, homogeneous and defect-free precursor layer is a prerequisite for adherent and reproducible copper structures. The knowledge of the rheological properties of an ink is crucial for the selection of a suitable coating technology as well as for the adjustment of the ink formulation. Different dilutions of the nanosuspension were examined for their rheological behavior by recording flow curves. A strong shear thinning behavior was found and the viscosity decreases exponentially with increasing dilution. The viscoelastic behavior was investigated by a simulated doctor blade coating process using three-interval thixotropy tests. An overshoot in viscosity is observed, which decreases with increasing thinning of the precursor. As a comparison to these results, doctor blade coating of planar glass and polymer substrates was performed to prepare precursor layers for reductive laser sintering. Surface morphology measurements of the resulting coatings using laser scanning microscopy and rheological tests show that homogeneous precursor layers with constant thickness can be produced at a particle–solvent ratio of 1.33. A too-high particle content results in an irregular coating layer with deep grooves and a peak-to-valley height Sz of up to 7.8 μm. Precise dilution control allows the fabrication of smooth surfaces with a Sz down to 1.5 μm. Full article
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15 pages, 17651 KiB  
Article
Preparation of Dispersed Copper(II) Oxide Nanosuspensions as Precursor for Femtosecond Reductive Laser Sintering by High-Energy Ball Milling
by Kay Bischoff, Cemal Esen and Ralf Hellmann
Nanomaterials 2023, 13(19), 2693; https://doi.org/10.3390/nano13192693 - 2 Oct 2023
Cited by 9 | Viewed by 1978
Abstract
This contribution demonstrates and discusses the preparation of finely dispersed copper(II) oxide nanosuspensions as precursors for reductive laser sintering (RLS). Since the presence of agglomerates interferes with the various RLS sub-processes, fine dispersion is required, and oversized particles must be identified by a [...] Read more.
This contribution demonstrates and discusses the preparation of finely dispersed copper(II) oxide nanosuspensions as precursors for reductive laser sintering (RLS). Since the presence of agglomerates interferes with the various RLS sub-processes, fine dispersion is required, and oversized particles must be identified by a measurement methodology. Aside from the established method of scanning electron microscopy for imaging individual dried particles, this work applies the holistic and statistically more significant laser diffraction in combination with dynamic image analysis in wet dispersion. In addition to direct ultrasonic homogenization, high-energy ball milling is introduced for RLS, to produce stable nanosuspensions with a high fine fraction, and, above all, the absence of oversize particles. Whereas ultrasonic dispersion stagnates at particle sizes between 500 nm and 20 μm, even after 8 h, milled suspension contains a high proportion of finest particles with diameters below 100 nm, no agglomerates larger than 1 μm and a trimodal particle size distribution with the median at 50 nm already, after 100 min of milling. The precursor layers produced by doctor blade coating are examined for their quality by laser scanning microscopy. The surface roughness of such a dry film can be reduced from 1.26 μm to 88 nm by milling. Finally, the novel precursor is used for femtosecond RLS, to produce homogeneous, high-quality copper layers with a sheet resistance of 0.28Ω/sq and a copper mass concentration of 94.2%. Full article
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15 pages, 4557 KiB  
Article
Fundamental Considerations and Analysis of the Energy Distribution in Laser Turning with Ultrashort Laser Pulses
by Julian Zettl, Cemal Esen and Ralf Hellmann
Micromachines 2023, 14(10), 1838; https://doi.org/10.3390/mi14101838 - 27 Sep 2023
Cited by 3 | Viewed by 1578
Abstract
This article discusses the process of the laser turning of rotational symmetric, cylindrical components using ultrashort laser pulses with respect to the geometrical conditions and the resulting energy distribution during the laser turning process. As a result, process predictions and potential process optimizations [...] Read more.
This article discusses the process of the laser turning of rotational symmetric, cylindrical components using ultrashort laser pulses with respect to the geometrical conditions and the resulting energy distribution during the laser turning process. As a result, process predictions and potential process optimizations are feasible. Particular attention is drawn to the laser spot formation on the cylindrical surface of the work piece in conjunction with the positioning of the laser beam relative to the rotation axis of the specimen. Based on fundamental calculations and experimental results, an optimum processing strategy is discussed, whereat the use of a trepanning optic in the laser turning process and the forming of a particular surface structure is additionally being issued. Full article
(This article belongs to the Special Issue Femtosecond Laser Micromachining)
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12 pages, 2479 KiB  
Article
Drilling Sequence Optimization Using Evolutionary Algorithms to Reduce Heat Accumulation for Femtosecond Laser Drilling with Multi-Spot Beam Profiles
by Christian Lutz, Jonas Helm, Katrin Tschirpke, Cemal Esen and Ralf Hellmann
Materials 2023, 16(17), 5775; https://doi.org/10.3390/ma16175775 - 23 Aug 2023
Cited by 9 | Viewed by 1943
Abstract
We report on laser drilling borehole arrays using ultrashort pulsed lasers with a particular focus on reducing the inadvertent heat accumulation across the workpiece by optimizing the drilling sequence. For the optimization, evolutionary algorithms are used and their results are verified by thermal [...] Read more.
We report on laser drilling borehole arrays using ultrashort pulsed lasers with a particular focus on reducing the inadvertent heat accumulation across the workpiece by optimizing the drilling sequence. For the optimization, evolutionary algorithms are used and their results are verified by thermal simulation using Comsol and experimentally evaluated using a thermal imaging camera. To enhance process efficiency in terms of boreholes drilled per second, multi-spot approaches are employed using a spatial light modulator. However, as higher temperatures occur across the workpiece when using simultaneous multi-spot drilling as compared to a single-spot process, a subtle spatial distribution and sequence of the multi-spot approach has to be selected in order to limit the resulting local heat input over the processing time. Different optimization approaches based on evolutionary algorithms aid to select those drilling sequences which allow for the combination of a high efficiency of multi-spot profiles, a low-generated process temperature and a high-component quality. In particular, using a 4 × 4 laser spot array allows for the drilling of 40,000 boreholes in less than 76 s (526 boreholes/s) with a reduced temperature increase by about 35%, as compared to a single spot process when employing an optimized drilling sequence. Full article
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14 pages, 35770 KiB  
Article
Static and Dynamic Mechanical Behaviour of Hybrid-PBF-LB/M-Built and Hot Isostatic Pressed Lattice Structures
by David Sommer, Cemal Esen and Ralf Hellmann
Materials 2023, 16(9), 3556; https://doi.org/10.3390/ma16093556 - 6 May 2023
Cited by 3 | Viewed by 2055
Abstract
We report on a comprehensive study of the mechanical properties of maraging steel body-centred cubic lattice structures fabricated by a hybrid additive manufacturing technology that combines laser powder bed fusion with in situ high-speed milling. As the mechanical properties of additive manufactured components [...] Read more.
We report on a comprehensive study of the mechanical properties of maraging steel body-centred cubic lattice structures fabricated by a hybrid additive manufacturing technology that combines laser powder bed fusion with in situ high-speed milling. As the mechanical properties of additive manufactured components are inferior to, e.g., cast components, surface modifications can improve the mechanical behaviour. Different hybrid additive manufacturing technologies have been designed using additive and subtractive processes, improving process quality. Following this, mechanical testing is performed with respect to static tensile properties and dynamic stress, hardness, and porosity, comparing specimens manufactured by laser powder bed fusion only to those manufactured by the hybrid approach. In addition, the influence of different heat-treatment techniques on the mechanical behaviour of the lattice structures is investigated, namely solution and aging treatment as well as hot isostatic pressing. Thus, the influence of the superior surface quality due to the hybrid approach is evaluated, leading to, e.g., an offset of about 14–16% for the static testing of HIP lattice structures. Furthermore, the dynamic load behaviour can be improved with a finished surface, heading to a shift of the different zones of fatigue behaviour in the testing of hybrid-built specimens. Full article
(This article belongs to the Special Issue Mechanical Properties of Polymeric, Metallic, and Composite Materials)
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9 pages, 5383 KiB  
Communication
Multi-Bessel Beams Generated by an Axicon and a Spatial Light Modulator for Drilling Applications
by Christian Lutz, Simon Schwarz, Jan Marx, Cemal Esen and Ralf Hellmann
Photonics 2023, 10(4), 413; https://doi.org/10.3390/photonics10040413 - 6 Apr 2023
Cited by 15 | Viewed by 3606
Abstract
We report on an optical setup to generate multi-Bessel beam profiles combining a refractive axicon and a spatial light modulator. Based on their particular beam profile, Bessel beams offer advantageous properties for micro drilling processes and internal volume processing, especially for transparent materials. [...] Read more.
We report on an optical setup to generate multi-Bessel beam profiles combining a refractive axicon and a spatial light modulator. Based on their particular beam profile, Bessel beams offer advantageous properties for micro drilling processes and internal volume processing, especially for transparent materials. In addition, the laser power of industrial, ultrashort pulsed lasers has increased significantly over the last few years, offering the possibility for highly efficient processes using multi-spot profiles. Our optical concept combines the dynamic possibilities of beam splitting using a spatial light modulator with the benefits of Bessel beams, which facilitates multi-Bessel beam processing. Beside the simulation and experimental evaluation of the generated multi-Bessel beams, we exemplify the applicability of the developed module for the perforation of thin metal foils by micro drilling. Full article
(This article belongs to the Special Issue Lasers and Dynamic of Systems)
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17 pages, 5614 KiB  
Article
Evaluation of a Cut Interruption Algorithm for Laser Cutting Steel and Aluminum with a High-Speed Camera
by Max Schleier, Cemal Esen and Ralf Hellmann
Appl. Sci. 2023, 13(7), 4557; https://doi.org/10.3390/app13074557 - 3 Apr 2023
Cited by 3 | Viewed by 2814
Abstract
We report on a monitoring system based on a high-speed camera for fiber laser fusion cutting. The monitoring system is used without an external illumination retrofit on a conventional cutting head, with the optical path aligned coaxially to the incident laser, permitting a [...] Read more.
We report on a monitoring system based on a high-speed camera for fiber laser fusion cutting. The monitoring system is used without an external illumination retrofit on a conventional cutting head, with the optical path aligned coaxially to the incident laser, permitting a direct, spatially, and temporally resolved detection of the melt pool area in the cut kerf from the top view. The dependence of the melt pool area on laser processing parameters such as laser power and feed rate are thus evaluated for stainless steel, zinc-coated steel, and aluminum, respectively. The signal characteristics of the images captured from the melt pool are examined in the visible spectral range of the emitted secondary thermal radiation from the process zone. An ad hoc developed image processing algorithm analyzes the spectral and geometric information of the melt pool from high-speed camera images and distinguishes between complete and incomplete cuts. Full article
(This article belongs to the Section Optics and Lasers)
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13 pages, 21103 KiB  
Article
Investigation of Topographical Alterations in Titanium-Zirconium-Alloy Implant Threads following Er:YAG Irradiation
by Mustafa Ayna, Johannes Spille, Yahya Açil, Jan-Tobias Weitkamp, Jörg Wiltfang, Cemal Esen and Aydin Gülses
Materials 2022, 15(22), 7889; https://doi.org/10.3390/ma15227889 - 8 Nov 2022
Cited by 3 | Viewed by 1461
Abstract
The aim of the current experimental study was to comparatively assess the surface alterations in titanium and titanium-zirconium alloy implants in terms of thread pitch topography after irradiation with an Er:YAG laser, which is recommended in the literature for its sterilizing effect in [...] Read more.
The aim of the current experimental study was to comparatively assess the surface alterations in titanium and titanium-zirconium alloy implants in terms of thread pitch topography after irradiation with an Er:YAG laser, which is recommended in the literature for its sterilizing effect in the treatment of contaminated implant surfaces. Roxolid® and SLA® (Sand-blasted, Large-grit, Acid-etched) implants from Straumann® company with the same macro topography were investigated. The surface treatment was carried out using a wavelength of 2940 nm, 60 s irradiation time, a frequency of 10 Hz, and energies between 120 mJ and 250 mJ. The alterations were quantitatively analyzed by conducting roughness analysis via white light interferometry and qualitatively using SEM images. Roxolid® could particularly maintain its surface topography at a level of 160 mJ. At an energy level of 250 mJ, the surface properties of the pitch could be significantly altered for the first time. Compared to the Standard Plus dental implants studied, no distinct removal of the material from the surface was detected. The alloy properties of Roxolid® confirm the manufacturer’s statement in terms of stability and could offer advantages in peri-implantitis management if decontamination has been selected. However, as a part of a respective strategy, smoothening of a Roxolid® implant surface requires a significantly higher energy level compared to SLA-Standard® dental implants. Full article
(This article belongs to the Section Metals and Alloys)
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11 pages, 4959 KiB  
Communication
Femtosecond Laser-Based Micromachining of Rotational-Symmetric Sapphire Workpieces
by Stefan Kefer, Julian Zettl, Cemal Esen and Ralf Hellmann
Materials 2022, 15(18), 6233; https://doi.org/10.3390/ma15186233 - 8 Sep 2022
Cited by 7 | Viewed by 2288
Abstract
Sapphire is a robust and wear-resistant material. However, efficient and high-quality micromachining is still a challenge. This contribution demonstrates and discusses two novels, previously unreported approaches for femtosecond laser-based micromachining of rotational-symmetric sapphire workpieces, whereas both methods are in principal hybrids of laser [...] Read more.
Sapphire is a robust and wear-resistant material. However, efficient and high-quality micromachining is still a challenge. This contribution demonstrates and discusses two novels, previously unreported approaches for femtosecond laser-based micromachining of rotational-symmetric sapphire workpieces, whereas both methods are in principal hybrids of laser scanning and laser turning or laser lathe. The first process, a combination of a sequential linear hatch pattern in parallel to the workpiece’s main axis with a defined incremental workpiece rotation, enables the fabrication of sapphire fibers with diameters of 50 μm over a length of 4.5 mm. Furthermore, sapphire specimens with a diameter of 25 μm over a length of 2 mm can be fabricated whereas an arithmetical mean height, i.e., Sa parameter, of 281 nm is achieved. The second process combines a constant workpiece feed and orthogonal scanning with incremental workpiece rotation. With this approach, workpiece length limitations of the first process are overcome and sapphire fibers with an average diameter of 90 µm over a length of 20 cm are manufactured. Again, the sapphire specimen exhibits a comparable surface roughness with an average Sa value of 249 nm over 20 cm. Based on the obtained results, the proposed manufacturing method paves an innovative and flexible, all laser-based way towards the fabrication or microstructuring of sapphire optical devices, and thus, a promising alternative to chemical processes. Full article
(This article belongs to the Special Issue Advances in Laser Processing)
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16 pages, 8251 KiB  
Article
UV-Femtosecond-Laser Structuring of Cyclic Olefin Copolymer
by Kay Bischoff, Dominik Mücke, Gian-Luca Roth, Cemal Esen and Ralf Hellmann
Polymers 2022, 14(14), 2962; https://doi.org/10.3390/polym14142962 - 21 Jul 2022
Cited by 10 | Viewed by 3260
Abstract
We report on the laser ablation of cyclic olefin copolymer using an amplified ultrashort pulsed laser in the ultraviolet spectral range. In addition to a high ablation depth per laser-structured layer up to 74 μm at a fluence of 22 J cm [...] Read more.
We report on the laser ablation of cyclic olefin copolymer using an amplified ultrashort pulsed laser in the ultraviolet spectral range. In addition to a high ablation depth per laser-structured layer up to 74 μm at a fluence of 22 J cm2, an excellent mean roughness Ra of laser-patterned surfaces down to 0.5 μm is demonstrated. Furthermore, with increasing fluence, increasing ablation efficiencies up to 2.5 mm3 W−1 min−1 are determined. Regarding the quality of the ablation, we observed steep ablation flanks and low debris formation, though for fluences above 10.5 J cm2 the formation of troughs was observed, being attributed to multiple reflections on the ablation flanks. For comparison, laser ablation was performed under identical conditions with an infrared laser wavelength. The results highlight that UV ablation exhibits significant advantages in terms of ablation efficiency, surface roughness and quality. Moreover, our results show that a larger UV focus spot accelerates the ablation process with comparable quality, paving the way for high-power UV ultrashort pulsed lasers towards an efficient and qualitative tool for the laser machining of cyclic olefin copolymer. The production of complex microfluidics further underlines the suitability of this type of laser. Full article
(This article belongs to the Section Polymer Processing and Engineering)
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12 pages, 2793 KiB  
Article
Optimization of Heat Accumulation during Femtosecond Laser Drilling Borehole Matrices by Using a Simplex Algorithm
by Christian Lutz, Marcel Jung, Katrin Tschirpke, Cemal Esen and Ralf Hellmann
Materials 2022, 15(14), 4829; https://doi.org/10.3390/ma15144829 - 11 Jul 2022
Cited by 2 | Viewed by 2172
Abstract
We report on an optimization study of percussion drilling thin metal sheets employing a high repetition rate, high power femtosecond laser with respect to the resulting heat accumulation. A specified simplex algorithm was employed to optimize the spatial drilling sequence, whereas a simplified [...] Read more.
We report on an optimization study of percussion drilling thin metal sheets employing a high repetition rate, high power femtosecond laser with respect to the resulting heat accumulation. A specified simplex algorithm was employed to optimize the spatial drilling sequence, whereas a simplified thermal simulation using COMSOL was validated by comparing its results to the temperature measurements using an infrared camera. Optimization for drilling borehole matrices was aspired with respect to the generated temperature across the processed specimen, while the drilling strategy was altered in its spatial drilling sequence and by using multi-spot approaches generated by a spatial light modulator. As a result, we found that an optimization strategy based on limited consecutive holes in a Moore neighborhood led to reduced temperatures and the shortest process times. Full article
(This article belongs to the Special Issue Advances in Laser Processing)
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13 pages, 19023 KiB  
Article
Ultrashort Pulsed Laser Drilling of Printed Circuit Board Materials
by Daniel Franz, Tom Häfner, Tim Kunz, Gian-Luca Roth, Stefan Rung, Cemal Esen and Ralf Hellmann
Materials 2022, 15(11), 3932; https://doi.org/10.3390/ma15113932 - 31 May 2022
Cited by 21 | Viewed by 4747
Abstract
We report on a comprehensive study of laser percussion microvia drilling of FR-4 printed circuit board material using ultrashort pulse lasers with emission in the green spectral region. Laser pulse durations in the pico- and femtosecond regime, laser pulse repetition rates up to [...] Read more.
We report on a comprehensive study of laser percussion microvia drilling of FR-4 printed circuit board material using ultrashort pulse lasers with emission in the green spectral region. Laser pulse durations in the pico- and femtosecond regime, laser pulse repetition rates up to 400 kHz and laser fluences up to 11.5 J/cm2 are applied to optimize the quality of microvias, as being evaluated by the generated taper, the extension of glass fiber protrusions and damage of inner lying copper layers using materialography. The results are discussed in terms of the ablation threshold for FR-4 and copper, heat accumulation and pulse shielding effects as a result of pulse to pulse interactions. As a specific result, using a laser pulse duration of 2 ps appears beneficial, resulting in small glass fiber protrusions and high precision in the stopping process at inner copper layer. If laser pulse repetition rates larger than 100 kHz are applied, we find that the processing quality can be increased by heat accumulation effects. Full article
(This article belongs to the Special Issue Advances in Laser Processing)
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14 pages, 7780 KiB  
Article
Image Processing Algorithm for In Situ Monitoring Fiber Laser Remote Cutting by a High-Speed Camera
by Max Schleier, Benedikt Adelmann, Cemal Esen and Ralf Hellmann
Sensors 2022, 22(8), 2863; https://doi.org/10.3390/s22082863 - 8 Apr 2022
Cited by 7 | Viewed by 3348
Abstract
We present an in situ process monitoring approach for remote fiber laser cutting, which is based on evaluating images from a high-speed camera. A specifically designed image processing algorithm allows the distinction between complete and incomplete cuts by analyzing spectral and geometric information [...] Read more.
We present an in situ process monitoring approach for remote fiber laser cutting, which is based on evaluating images from a high-speed camera. A specifically designed image processing algorithm allows the distinction between complete and incomplete cuts by analyzing spectral and geometric information of the melt pool from the captured images of the high-speed camera. The camera-based monitoring system itself is fit to a conventional laser deflection unit for use with high-power fiber lasers, with the optical detection path being coaxially aligned to the incident laser. Without external illumination, the radiation of the melt from the process zone is recorded in the visible spectral range from the top view and spatially and temporally resolved. The melt pool size and emitted sparks are evaluated in dependence of machining parameters such as feed rate, cycles, and focus position during cutting electrical sheets. Full article
(This article belongs to the Section Sensing and Imaging)
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13 pages, 1807 KiB  
Article
Tool Wear and Milling Characteristics for Hybrid Additive Manufacturing Combining Laser Powder Bed Fusion and In Situ High-Speed Milling
by David Sommer, Dominik Pape, Cemal Esen and Ralf Hellmann
Materials 2022, 15(3), 1236; https://doi.org/10.3390/ma15031236 - 7 Feb 2022
Cited by 13 | Viewed by 2828
Abstract
We report on milling and tool wear characteristics of hybrid additive manufacturing comprising laser powder bed fusion and in situ high-speed milling, a particular process in which the cutter mills inside the powder bed without any cooling lubricant being applicable. Flank wear is [...] Read more.
We report on milling and tool wear characteristics of hybrid additive manufacturing comprising laser powder bed fusion and in situ high-speed milling, a particular process in which the cutter mills inside the powder bed without any cooling lubricant being applicable. Flank wear is found to be the dominant wear characteristic with its temporal evolution over utilization period revealing the typical s-shaped dependence. The flank wear land width is measured by microscopy and correlated to the achievable surface roughness of milled 3D-printed parts, showing that for flank wear levels up to 100 μm a superior surface roughness below 3 μm is accessible for hybrid additive manufacturing. Further, based on this correlation recommended tool, life scenarios can be deduced. In addition, by optimizing the finishing tool start position and the number of afore-built layers, the milling process is improved with respect to the maximum millable angle for undercut surfaces of 3D-printed parts to 30° for the roughing process and to 40° for the entire machining process including finishing. Full article
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