Development of Edible Composite Film from Fish Gelatin–Pectin Incorporated with Lemongrass Essential Oil and Its Application in Chicken Meat
Abstract
:1. Introduction
2. Materials and Methods
2.1. Material
2.2. Edible Film Preparation
2.3. Thickness
2.4. Color
2.5. Water Content and Film Solubility
2.6. Transmittance and Transparency
2.7. Mechanical Properties (Tensile Strength and Elongation at Break)
2.8. Fourier Transform Infrared (FTIR) Spectra
2.9. Antioxidant Activities
2.10. Antibacterial Activities
2.11. Water Contact Angle Measurements
2.12. Microstructure Analysis of Films
2.13. Thermal Properties
2.14. Application of Edible Film in Breast Meat Fillet
3. Results and Discussion
3.1. Thickness
3.2. Color
3.3. Water Content and Solubility
3.4. Transmittance and Transparency
3.5. Mechanical Properties (Tensile Strength and Elongation at Break)
3.6. Fourier Transform Infrared Spectroscopy (FTIR)
3.7. Antioxidant Activities
3.8. Antibacterial Activities
3.9. Water Contact Angle
3.10. Microstructure of Films
3.11. Thermal Properties
3.12. Application of Edible Film in Breast Meat Fillet
3.12.1. Moisture Content
3.12.2. PH Values
3.12.3. Hardness
3.12.4. Color Values
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Formula of Biocomposite | Concentration of Lemongrass | Concentration of Glycerol | Sample Code |
---|---|---|---|
Gelatin 100% Pectin 0% | 0% | 25% | G100 |
0.5% | 25% | G100M05 | |
Gelatin 75% Pectin 25% | 0% | 25% | G75 |
0.50% | 25% | G75M05 | |
Gelatin 50% Pectin 50% | 0% | 25% | G50 |
0.5% | 25% | G50M05 |
Sample | Color | ||
---|---|---|---|
L* | a* | b* | |
G100 | 93.11 d ± 0.1 | −7.68 b ± 0.16 | 4.52 a ± 0.11 |
G75 | 91.72 bc ± 0.6 | −7.89 a ± 0.03 | 5.33 b ± 0.20 |
G50 | 91.61 bc ± 0.15 | −7.96 a ± 0.02 | 6.56 c ± 0.32 |
G100M05 | 91.97 c ± 0.57 | −4.83 c ± 0.04 | 4.18 a ± 0.07 |
G75M05 | 91.21 ab ± 0.09 | −4.55 d ± 0.14 | 5.14 b ± 0.31 |
G50M05 | 90.6 a ± 0.07 | −4.03 e ± 0.07 | 5.24 b ± 0.57 |
Sample | Water Content (%) | Solubility (%) |
---|---|---|
G100 | 18.63 a ± 0.58 | 89.11 d ± 5.6 |
G75 | 21.78 c ± 0.18 | 69.18 c ± 2.8 |
G50 | 23.11 d ± 0.13 | 60.96 b ± 3.26 |
G100M05 | 19.57 b ± 0.36 | 71.16 c ± 1.15 |
G75M05 | 22.42 c ± 0.46 | 48.23 a ± 1.48 |
G50M05 | 23.57 d ± 0.28 | 56.87 b ± 1.45 |
Sample | Transparency |
---|---|
G100 | 3.82 d ± 0.052 |
G75 | 3.69 c ± 0.101 |
G50 | 3.51 b ± 0.025 |
G100M05 | 3.60 b ± 0.017 |
G75M05 | 3.69 c ± 0.105 |
G50M05 | 3.39 a ± 0.023 |
Sample | Tensile Strength (MPa) | Elongation at Break (%) |
---|---|---|
G100 | 9.55 a ± 3.93 | 75.01 cd ± 5.86 |
G75 | 6.37 a ± 3.99 | 54.75 b ± 17.46 |
G50 | 7.22 a ± 0.75 | 24.96 a ± 2.60 |
G100M05 | 14.17 a ± 1.49 | 86.13 d ± 1.75 |
G75M05 | 6.40 a ± 1.14 | 66.29 bc ± 16.37 |
G50M05 | 6.49 b ± 0.97 | 30.98 a ± 3.19 |
Sample | Antioxidant Activity (%RSA) |
---|---|
G100 | 6.36 a ± 0.14 |
G75 | 11.84 b ± 0.14 |
G50 | 23.48 e ± 0.28 |
G100M05 | 13.25 c ± 0.20 |
G75M05 | 24.20 f ± 0.10 |
G50M05 | 20.36 d ± 0.20 |
Sample | Inhibition Zone (mm) | |
---|---|---|
S. aureus | Salmonella | |
G100 | 0 | 0 |
G75 | 0 | 0 |
G50 | 0 | 0 |
G100M05 | 0 | 0 |
G75M05 | 0 | 9 |
G50M05 | 0 | 14 |
Sample | Onset Temperature (°C) | Peak Temperature (°C) | ∆H (J/g) |
---|---|---|---|
G100 | 130.98 | 131.65 | −2.61 |
G75 | 139.39 | 142.94 | −190.86 |
G50 | 162.78 | 163.72 | −73.74 |
G100M05 | 170.96 | 171.71 | −9.39 |
G75M05 | 177.66 | 179.06 | −269.69 |
G50M05 | 173.88 | 176.64 | −42.59 |
Parameters | Days | Control | PE | G75M05 | G50M05 |
---|---|---|---|---|---|
Moisture content (%) | 0 | 75.34 ± 0.21 dA | 75.37 ± 0.26 dD | 75.48 ± 0.24 dB | 75.09 ± 0.79 dC |
2 | 60.85 ± 0.77 cA | 74.48 ± 0.07 cD | 62.65 ± 0.94 cB | 64.89 ± 0.66 cC | |
4 | 54.89 ± 0.73 bA | 74.29 ± 0.29 bD | 58.00 ± 0.74 bB | 61.6 ± 0.35 bC | |
6 | 44.12 ± 0.59 aA | 74.85 ± 0.11 aD | 46.38 ± 0.52 aB | 53.09 ± 0.3 aC | |
PH | 0 | 5.74 ± 0.09 bC | 5.75 ± 0.02 bD | 5.81 ± 0.02 bB | 5.8 ± 0.01 bA |
2 | 5.63 ± 0.07 aC | 6.03 ± 0.07 aD | 5.68 ± 0.06 aB | 5.51 ± 0.03 aA | |
4 | 5.99 ± 0.15 cC | 6.44 ± 0.01 cD | 5.57 ± 0.02 cB | 5.43 ± 0.03 cA | |
6 | 6.45 ± 0.04 dC | 6.49 ± 0.03 dD | 5.67 ± 0.04 dB | 5.72 ± 0.07 dA | |
Hardness (N) | 0 | 0.63 ± 0.06 aC | 0.5 ± 0.03 aA | 0.46 ± 0.04 aB | 0.49 ± 0.07 aB |
2 | 0.99 ± 0.05 bC | 0.61 ± 0.01 bA | 0.67 ± 0.05 bB | 0.62 ± 0.02 bB | |
4 | 1.15 ± 0.04 bC | 0.37 ± 0.04 bA | 0.73 ± 0.01 bB | 0.74 ± 0.08 bB | |
6 | 2.27 ± 0.11 cC | 0.36 ± 0.04 cA | 1.06 ± 0.04 cB | 1.07 ± 0.07 cB | |
L* | 0 | 53.82 ± 0.41 dA | 51.16 ± 0.86 dC | 54.52 ± 0.97 dA | 54.4 ± 0.69 dB |
2 | 42.11 ± 1.59 cA | 49.51 ± 1.13 cC | 38.29 ± 1.39 cA | 42.97 ± 1.97 cB | |
4 | 37.66 ± 1.51 bA | 43.62 ± 1.38 bC | 38.98 ± 2.5 bA | 41.17 ± 2 bB | |
6 | 30.41 ± 0.12 aA | 47.94 ± 0.24 aC | 36.07 ± 0.2 aA | 36.55 ± 0.08 aB | |
a* | 0 | −2.23 ± 0.11 aD | −2.3 ± 0.09 aA | −2.21 ± 0.1 aC | −2.34 ± 0.18 aB |
2 | 1.19 ± 0.04 bD | 1.32 ± 0.08 bA | −1.97 ± 0.69 bC | −1.94 ± 0.29 bB | |
4 | 2.35 ± 0.08 cD | −1.27 ± 0.15 cA | 2.09 ± 0.55 cC | 1.19 ± 0.02 cB | |
6 | 3.02 ± 0.17 cD | −1.57 ± 0.16 cA | 1.82 ± 0.69 cC | 1.79 ± 0.07 cB | |
b* | 0 | 11.22 ± 0.11 aB | 11.53 ± 0.71 aA | 11.66 ± 0.85 aC | 9.57 ± 1.47 aB |
2 | 12.51 ± 0.42 bB | 9.29 ± 0.92 bA | 13.32 ± 0.7 bC | 11.85 ± 0.8 bB | |
4 | 13.57 ± 0.58 bB | 7.27 ± 0.51 bA | 14.36 ± 0.69 bC | 13.27 ± 0.81 bB | |
6 | 9.92 ± 0.03 aB | 7.57 ± 0.21 aA | 13.54 ± 0.06 aC | 13.29 ± 0.09 aB |
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Azizah, F.; Nursakti, H.; Ningrum, A.; Supriyadi. Development of Edible Composite Film from Fish Gelatin–Pectin Incorporated with Lemongrass Essential Oil and Its Application in Chicken Meat. Polymers 2023, 15, 2075. https://doi.org/10.3390/polym15092075
Azizah F, Nursakti H, Ningrum A, Supriyadi. Development of Edible Composite Film from Fish Gelatin–Pectin Incorporated with Lemongrass Essential Oil and Its Application in Chicken Meat. Polymers. 2023; 15(9):2075. https://doi.org/10.3390/polym15092075
Chicago/Turabian StyleAzizah, Farrah, Herwinda Nursakti, Andriati Ningrum, and Supriyadi. 2023. "Development of Edible Composite Film from Fish Gelatin–Pectin Incorporated with Lemongrass Essential Oil and Its Application in Chicken Meat" Polymers 15, no. 9: 2075. https://doi.org/10.3390/polym15092075