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Crystals 2016, 6(1), 13; doi:10.3390/cryst6010013

Crystal Structures of Two 1,4-Diamino-1,2,4-triazolium Salts

1
Faculty of Chemistry and Pharmacy, University of Innsbruck, 6020 Innsbruck, Austria
2
Institute of Mineralogy and Petrography, University of Innsbruck, 6020 Innsbruck, Austria
*
Author to whom correspondence should be addressed.
Academic Editor: Helmut Cölfen
Received: 30 December 2015 / Revised: 13 January 2016 / Accepted: 18 January 2016 / Published: 20 January 2016
(This article belongs to the Special Issue Nitrogen-Rich Salts)
View Full-Text   |   Download PDF [1570 KB, uploaded 20 January 2016]   |  

Abstract

Bis(1,4-diamino-1,2,4-triazolium) sulfate (1) was obtained from the corresponding chloride by ion metathesis using Ag2SO4. Further metathesis with barium 5,5′-azotetrazolate yielded bis(1,4-diamino-1,2,4-triazolium) 5,5′-azotetrazolate (2). Numerous NH···N and NH···O interactions were identified in the crystal structures of 1 and 2. Both compounds undergo exothermal decomposition upon heating. View Full-Text
Keywords: azotetrazolate; hydrogen bond; sulfate; thermoanalysis; triazolium azotetrazolate; hydrogen bond; sulfate; thermoanalysis; triazolium
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (CC BY 4.0).

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MDPI and ACS Style

Laus, G.; Wurst, K.; Kahlenberg, V.; Schottenberger, H. Crystal Structures of Two 1,4-Diamino-1,2,4-triazolium Salts. Crystals 2016, 6, 13.

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