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Crystals 2015, 5(1), 9-13; doi:10.3390/cryst5010009

Synthesis and Molecular Structure of 2-(Diphenylphosphano)phenyl Benzoate Borane Adduct

1
Institut für Radiopharmazie, Helmholtz-Zentrum Dresden-Rossendorf, Bautzner Landstraße 400, D-01328 Dresden, Germany
2
Institut für Chemie, Universität Rostock, Anorganische Festkörperchemie, Albert-Einstein-Straße 3a, D-18059 Rostock, Germany
*
Author to whom correspondence should be addressed.
Academic Editor: Nikolaus Korber
Received: 5 November 2014 / Accepted: 12 December 2014 / Published: 29 December 2014
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Abstract

The crystal and molecular structure of 2-(diphenylphosphano)phenyl benzoate borane adduct are reported. The title compound crystallizes from a petroleum ether/ethyl acetate mixture in the triclinic space group P with two molecules in the unit cell. The unit cell parameters are: a = 8.67(1) Å, b = 9.202(1) Å, c = 14.224(2) Å; α = 72.600(7)°, β = 73.577(7)°, γ = 84.349(7)° and V = 1039.5(2) Å3. Bond lengths and angles are typical for this phosphane borane adduct. View Full-Text
Keywords: building block; Lewis acid-base; Staudinger Ligation building block; Lewis acid-base; Staudinger Ligation
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This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (CC BY 4.0).

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MDPI and ACS Style

Mamat, C.; Köckerling, M. Synthesis and Molecular Structure of 2-(Diphenylphosphano)phenyl Benzoate Borane Adduct. Crystals 2015, 5, 9-13.

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