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Crystals 2013, 3(2), 333-338; doi:10.3390/cryst3020333
Short Note

The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate

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Received: 14 January 2013; in revised form: 6 March 2013 / Accepted: 13 May 2013 / Published: 17 May 2013
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Abstract: A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic space group P-1 with unit cell parameters a = 8.3801(11) Å; b = 9.2583(12) Å; c = 11.5671(15) Å; α = 73.566(2)°; β = 84.514(2)°; γ = 66.578(2)°. The asymmetric unit contains two molecules.
Keywords: dopamine; hydroxypyridinone; ligand; X-ray dopamine; hydroxypyridinone; ligand; X-ray
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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MDPI and ACS Style

Hall, S.R.; Roy, R.; McLaughlin, D.T.; Sullivan, K.J.; Barclay, L.R.C.; Vogels, C.M.; Decken, A.; Westcott, S.A. The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate. Crystals 2013, 3, 333-338.

AMA Style

Hall SR, Roy R, McLaughlin DT, Sullivan KJ, Barclay LRC, Vogels CM, Decken A, Westcott SA. The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate. Crystals. 2013; 3(2):333-338.

Chicago/Turabian Style

Hall, Steven R.; Roy, Raymond; McLaughlin, Dylan T.; Sullivan, Kate J.; Barclay, L. R.C.; Vogels, Christopher M.; Decken, Andreas; Westcott, Stephen A. 2013. "The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate." Crystals 3, no. 2: 333-338.

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