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Materials 2015, 8(3), 914-931; doi:10.3390/ma8030914

Characterization of Low-Symmetry Structures from Phase Equilibrium of Fe-Al System—Microstructures and Mechanical Properties

Department of Advanced Materials and Technologies, Faculty of Advanced Technologies and Chemistry, Military University of Technology, Gen. S. Kaliskiego 2 St., Warsaw 00-908, Poland
Author to whom correspondence should be addressed.
Academic Editor: Marco Salerno
Received: 20 December 2014 / Revised: 12 February 2015 / Accepted: 15 February 2015 / Published: 4 March 2015
(This article belongs to the Special Issue Intermetallic Alloys: Fabrication, Properties and Applications)
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Fe-Al intermetallic alloys with aluminum content over 60 at% are in the area of the phase equilibrium diagram that is considerably less investigated in comparison to the high-symmetry Fe3Al and FeAl phases. Ambiguous crystallographic information and incoherent data referring to the phase equilibrium diagrams placed in a high-aluminum range have caused confusions and misinformation. Nowadays unequivocal material properties description of FeAl2, Fe2Al5 and FeAl3 intermetallic alloys is still incomplete. In this paper, the influence of aluminum content and processing parameters on phase composition is presented. The occurrence of low-symmetry FeAl2, Fe2Al5 and FeAl3 structures determined by chemical composition and phase transformations was defined by scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS) examinations. These results served to verify diffraction investigations (XRD) and to explain the mechanical properties of cast materials such as: hardness, Young’s modulus and fracture toughness evaluated using the nano-indentation technique. View Full-Text
Keywords: Al-Fe alloy; microstructure; mechanical properties; SEM/EDS; XRD; nano-indentation Al-Fe alloy; microstructure; mechanical properties; SEM/EDS; XRD; nano-indentation

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This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (CC BY 4.0).

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MDPI and ACS Style

Matysik, P.; Jóźwiak, S.; Czujko, T. Characterization of Low-Symmetry Structures from Phase Equilibrium of Fe-Al System—Microstructures and Mechanical Properties. Materials 2015, 8, 914-931.

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