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Molbank 2012, 2012(4), M790; doi:10.3390/M790
Short Note

5-(tert-Butyldimethylsilyloxy)-1-(2-chloro-5,8-dimethoxyquinolin-3-yl)-3-methylenepentan-1-ol

1, 1,*  and 2
Received: 30 October 2012 / Accepted: 4 December 2012 / Published: 14 December 2012
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Abstract

Novel 5-(tert-butyldimethylsilyloxy)-1-(2-chloro-5,8-dimethoxyquinolin-3-yl)-3-methylenepentan-1-ol (7) was prepared via allylation of 2-chloro-5,8-dimethoxyquinoline-3-carbaldehyde (6) with functionalized allylic iodide as tert-butyl-(3-(iodomethyl)but-3-enyloxy)dimethylsilane (5), in the presence of metallic indium in anhydrous DMF as solvent at ambient temperature. The structure of the synthesized compound was assigned on the basis of elemental analysis and spectral data.
Keywords: functionalized allylic iodide; allylation; indium; quinoline derivatives functionalized allylic iodide; allylation; indium; quinoline derivatives
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Bouarata, L.; Tebbani, D.; Mosset, P. 5-(tert-Butyldimethylsilyloxy)-1-(2-chloro-5,8-dimethoxyquinolin-3-yl)-3-methylenepentan-1-ol. Molbank 2012, 2012, M790.

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