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Molbank 2011, 2011(4), M745; doi:10.3390/M745

Ethyl 4,4''-Difluoro-5'-hydroxy-1,1':3',1''-terphenyl-4'-carboxylate

1
Department of Studies in Chemistry, Mangalore University, Mangalagangotri-574 199, Karnataka, India
2
Research Department of Chemistry, P. A College of Engineering, Nadupadavu, Mangalore 574153, Karnataka, India
*
Author to whom correspondence should be addressed.
Received: 3 August 2011 / Accepted: 18 November 2011 / Published: 23 November 2011
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Abstract

A simple and novel route for the synthesis of new terphenyl derivative as well as oxidative aromatization of α,β-unsaturated cyclohexenone to the corresponding phenol derivative is developed. The present work involves the condensation of ethylacetoacetate with 4,4'-difluoro chalcone followed by the aromatization using chloramine-T in acetic acid to yield the title compound (3). The synthesized compound (3) is well characterized by IR, NMR, LCMS and elemental analysis.
Keywords: 4,4'-difluoro chalcone; cyclohexenone derivative; aromatization; chloramine-T; terphenyl derivative 4,4'-difluoro chalcone; cyclohexenone derivative; aromatization; chloramine-T; terphenyl derivative
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MDPI and ACS Style

Samshuddin, S.; Narayana, B.; Sarojini, B.K. Ethyl 4,4''-Difluoro-5'-hydroxy-1,1':3',1''-terphenyl-4'-carboxylate. Molbank 2011, 2011, M745.

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